N-(2,3-dihydro-1H-inden-5-yl)-N--N-(2,2,2-trichloroethoxycarbonyl)-L-alanyl>-glycine t-butyl ester

Base Information

Chemical Name:N-(2,3-dihydro-1H-inden-5-yl)-N--N-(2,2,2-trichloroethoxycarbonyl)-L-alanyl>-glycine t-butyl ester
CAS No.:101843-77-0
Molecular Formula:C₃₃H₄₁Cl₃N₂O₇
Molecular Weight:684.057
Hs Code.:

N-(2,3-dihydro-1H-inden-5-yl)-N-<N-<(1S)-1-(ethoxycarbonyl)-3-phenylpropyl>-N-(2,2,2-trichloroethoxycarbonyl)-L-alanyl>-glycine t-butyl ester

Synonyms:N-(2,3-dihydro-1H-inden-5-yl)-N--N-(2,2,2-trichloroethoxycarbonyl)-L-alanyl>-glycine t-butyl ester

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Chemical Property of N-(2,3-dihydro-1H-inden-5-yl)-N--N-(2,2,2-trichloroethoxycarbonyl)-L-alanyl>-glycine t-butyl ester

Chemical Property:

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Technology Process of N-(2,3-dihydro-1H-inden-5-yl)-N--N-(2,2,2-trichloroethoxycarbonyl)-L-alanyl>-glycine t-butyl ester

There total 4 articles about N-(2,3-dihydro-1H-inden-5-yl)-N--N-(2,2,2-trichloroethoxycarbonyl)-L-alanyl>-glycine t-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5292-43-3
bromoacetic acid tert-butyl ester

: 101843-77-0
N-(2,3-dihydro-1H-inden-5-yl)-N--N-(2,2,2-trichloroethoxycarbonyl)-L-alanyl>-glycine t-butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / propan-2-ol

2: 1.) oxalyl chloride, DMF; 2.) pyridine / 1.) methylene chloride, 2 h, room temp.; 2.) methylene chloride, 16 h

With pyridine; oxalyl dichloride; triethylamine; N,N-dimethyl-formamide; In isopropyl alcohol;

Reference yield:

: 24425-40-9
indan-5-amine

: 101843-77-0
N-(2,3-dihydro-1H-inden-5-yl)-N--N-(2,2,2-trichloroethoxycarbonyl)-L-alanyl>-glycine t-butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / propan-2-ol

2: 1.) oxalyl chloride, DMF; 2.) pyridine / 1.) methylene chloride, 2 h, room temp.; 2.) methylene chloride, 16 h

With pyridine; oxalyl dichloride; triethylamine; N,N-dimethyl-formamide; In isopropyl alcohol;

Reference yield:

: 80828-38-2
N-<(S)-1-(ethoxycarbonyl)-3-phenylpropyl>-L-alanine tert-butylester

: 101843-77-0
N-(2,3-dihydro-1H-inden-5-yl)-N--N-(2,2,2-trichloroethoxycarbonyl)-L-alanyl>-glycine t-butyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 99 percent / pyridine / tetrahydrofuran / 3 h / Heating

2: 76 percent / 4N HCl / dioxane / 8 h / Ambient temperature

3: 1.) oxalyl chloride, DMF; 2.) pyridine / 1.) methylene chloride, 2 h, room temp.; 2.) methylene chloride, 16 h

With pyridine; hydrogenchloride; oxalyl dichloride; N,N-dimethyl-formamide; In tetrahydrofuran; 1,4-dioxane;