C₂₄H₁₉BO

Base Information

• Chemical Name: C₂₄H₁₉BO
• CAS No.: 279216-31-8
• Molecular Formula: C₂₄H₁₉BO
• Molecular Weight: 334.225
• Mol file: 279216-31-8.mol

Synonyms:C₂₄H₁₉BO

Chemical Property of C₂₄H₁₉BO

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₄H₁₉BO

There total 5 articles about C₂₄H₁₉BO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(diethylamino)borane (18494-92-3) + 4-iodo-biphenyl (1591-31-7) + water (7732-18-5) → C24H19BO (279216-31-8)

Guidance literature:

(diethylamino)borane; 4-iodo-biphenyl; With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; N-ethyl-N,N-diisopropylamine; 1,3-bis-(2,6-diisopropylphenyl)-imidazol-2-ylidene; In toluene; at 100 ℃; for 24h; Glovebox; Inert atmosphere; Sealed tube;

water; With ammonium chloride; In toluene; at 0 - 20 ℃; for 0.75h; Glovebox; Inert atmosphere; Sealed tube;

DOI:10.1246/CL.200213

Reference yield:

C30H32BN + water (7732-18-5) → C24H19BO (279216-31-8)

Guidance literature:

With hydrogenchloride; In methanol; for 1h; Inert atmosphere;

DOI:10.1055/s-0036-1588345

Reference yield:

4-bromo-1,1'-biphenyl (92-66-0) + diisopropopylaminoborane (22092-92-8) → C24H19BO (279216-31-8)

Guidance literature:

With magnesium; In tetrahydrofuran; at 70 ℃; for 20h;

DOI:10.1021/acs.orglett.5b01620

upstream raw materials:

bis(biphenyl-4-yl)isopropoxyborane

4-bromo-1,1'-biphenyl

diisopropopylaminoborane

water

Downstream raw materials:

biphenyl

1-[1,1';4',1'']terphenyl-4-yl-ethanone