(S)-2-(2,4-dimethoxyphenyl)-3-(4-methoxy-2-O-methoxymethylphenyl)-1-propanol

Base Information

• Chemical Name: (S)-2-(2,4-dimethoxyphenyl)-3-(4-methoxy-2-O-methoxymethylphenyl)-1-propanol
• CAS No.: 225089-93-0
• Molecular Formula: C₂₀H₂₆O₆
• Molecular Weight: 362.423

Synonyms:(S)-2-(2,4-dimethoxyphenyl)-3-(4-methoxy-2-O-methoxymethylphenyl)-1-propanol

Chemical Property of (S)-2-(2,4-dimethoxyphenyl)-3-(4-methoxy-2-O-methoxymethylphenyl)-1-propanol

Chemical Property:

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Technology Process of (S)-2-(2,4-dimethoxyphenyl)-3-(4-methoxy-2-O-methoxymethylphenyl)-1-propanol

There total 3 articles about (S)-2-(2,4-dimethoxyphenyl)-3-(4-methoxy-2-O-methoxymethylphenyl)-1-propanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

(+)-(4S,5R)-1,5-dimethyl-4-phenyl-3-<2'-(2,4-dimethoxyphenyl)-3'-(4-methoxy-2-O-methoxymethylphenyl)>propionyl-2-imidazolidinone (225089-88-3) → (S)-2-(2,4-dimethoxyphenyl)-3-(4-methoxy-2-O-methoxymethylphenyl)-1-propanol (225089-93-0)

Guidance literature:

With lithium borohydride; In tetrahydrofuran; diethyl ether; for 18h; Ambient temperature;

DOI:10.1016/S0040-4020(98)01147-8

Reference yield:

4-methoxy-2-O-methoxymethylbenzyl bromide (152955-15-2) → (S)-2-(2,4-dimethoxyphenyl)-3-(4-methoxy-2-O-methoxymethylphenyl)-1-propanol (225089-93-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 1) lithium isopropylcyclohexylamide / 1) THF, -78 deg C to -50 deg C, 2) THF, DCM, -30 deg C, 8 h

2: 80 percent / LiBH₄ / diethyl ether; tetrahydrofuran / 18 h / Ambient temperature

With lithium borohydride; lithium cyclohexylisopropylamide; In tetrahydrofuran; diethyl ether;

DOI:10.1016/S0040-4020(98)01147-8

Reference yield:

(+)-(4S,5R)-1,5-dimethyl-4-phenyl-3-(2,4-dimethoxyphenylacetyl)-2-imidazolidinone (225089-83-8) → (S)-2-(2,4-dimethoxyphenyl)-3-(4-methoxy-2-O-methoxymethylphenyl)-1-propanol (225089-93-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 1) lithium isopropylcyclohexylamide / 1) THF, -78 deg C to -50 deg C, 2) THF, DCM, -30 deg C, 8 h

2: 80 percent / LiBH₄ / diethyl ether; tetrahydrofuran / 18 h / Ambient temperature

With lithium borohydride; lithium cyclohexylisopropylamide; In tetrahydrofuran; diethyl ether;

DOI:10.1016/S0040-4020(98)01147-8

upstream raw materials:

(+)-(4S,5R)-1,5-dimethyl-4-phenyl-3-<2'-(2,4-dimethoxyphenyl)-3'-(4-methoxy-2-O-methoxymethylphenyl)>propionyl-2-imidazolidinone

4-methoxy-2-O-methoxymethylbenzyl bromide

(+)-(4S,5R)-1,5-dimethyl-4-phenyl-3-(2,4-dimethoxyphenylacetyl)-2-imidazolidinone

Downstream raw materials:

(S)-7,2',4'-trimethoxyisoflavan

2-[(S)-2-(2,4-Dimethoxy-phenyl)-3-hydroxy-propyl]-5-methoxy-phenol

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