1-(3-(1H-1,2,4-triazol-1-yl)-4-(3,4,5-trimethoxybenzoyl)phenyl)-2-bromoethanone

Base Information

• Chemical Name: 1-(3-(1H-1,2,4-triazol-1-yl)-4-(3,4,5-trimethoxybenzoyl)phenyl)-2-bromoethanone
• CAS No.: 1016544-80-1
• Molecular Formula: C₂₀H₁₈BrN₃O₅
• Molecular Weight: 460.284

Synonyms:1-(3-(1H-1,2,4-triazol-1-yl)-4-(3,4,5-trimethoxybenzoyl)phenyl)-2-bromoethanone

Chemical Property of 1-(3-(1H-1,2,4-triazol-1-yl)-4-(3,4,5-trimethoxybenzoyl)phenyl)-2-bromoethanone

Chemical Property:

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Technology Process of 1-(3-(1H-1,2,4-triazol-1-yl)-4-(3,4,5-trimethoxybenzoyl)phenyl)-2-bromoethanone

There total 1 articles about 1-(3-(1H-1,2,4-triazol-1-yl)-4-(3,4,5-trimethoxybenzoyl)phenyl)-2-bromoethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

(4-(1-ethoxyvinyl)-2-(1H-1,2,4-triazol-1-yl)phenyl)(3,4,5-trimethoxyphenyl)methanone (1016544-79-8) → 1-(3-(1H-1,2,4-triazol-1-yl)-4-(3,4,5-trimethoxybenzoyl)phenyl)-2-bromoethanone (1016544-80-1)

Guidance literature:

With N-Bromosuccinimide; In tetrahydrofuran; water; at 20 ℃; for 2h;

DOI:10.1021/jm1002414

Reference yield: 48.0%

1-(3-(1H-1,2,4-triazol-1-yl)-4-(3,4,5-trimethoxybenzoyl)phenyl)-2-bromoethanone (1016544-80-1) + acetylguanidine (5699-40-1) → N-(4-(3-(1H-1,2,4-triazol-1-yl)-4-(3,4,5-trimethoxybenzoyl)phenyl)-1H-imidazol-2-yl)acetamide (1016543-82-0)

Guidance literature:

In acetonitrile; at 20 - 90 ℃; for 3h;

Reference yield: 48.0%

1-(3-(1H-1,2,4-triazol-1-yl)-4-(3,4,5-trimethoxybenzoyl)phenyl)-2-bromoethanone (1016544-80-1) + thiourea (17356-08-0) → (4-(2-aminothiazole-4-yl)-2-(1H-1,2,4-triazole-1-yl)phenyl)(3,4,5-trimethoxyphenyl)methanone (1016543-77-3)

Guidance literature:

In ethanol; for 2h; Heating / reflux;

upstream raw materials:

(4-(1-ethoxyvinyl)-2-(1H-1,2,4-triazol-1-yl)phenyl)(3,4,5-trimethoxyphenyl)methanone

Downstream raw materials:

N-(4-(3-(1H-1,2,4-triazol-1-yl)-4-(3,4,5-trimethoxybenzoyl)phenyl)-1H-imidazol-2-yl)acetamide

(4-(2-aminothiazole-4-yl)-2-(1H-1,2,4-triazole-1-yl)phenyl)(3,4,5-trimethoxyphenyl)methanone

(4-(2-methylthiazol-4-yl)-2-(1H-1,2,4-triazol-1-yl)phenyl)(3,4,5-trimethoxyphenyl)methanone

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