1,3-bis(mesityl)imidazolium hydrogen carbonate

Base Information

• Chemical Name: 1,3-bis(mesityl)imidazolium hydrogen carbonate
• CAS No.: 1372124-93-0
• Molecular Formula: CHO₃*C₂₁H₂₅N₂
• Molecular Weight: 366.46

Synonyms:1,3-bis(mesityl)imidazolium hydrogen carbonate

Chemical Property of 1,3-bis(mesityl)imidazolium hydrogen carbonate

Chemical Property:

Purity/Quality:

99%+ ^*data from raw suppliers

1,3-Bis(2,4,6-trimethylphenyl)imidazolium bicarbonate, min. 97% IMesH.HCO3 ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
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Technology Process of 1,3-bis(mesityl)imidazolium hydrogen carbonate

There total 1 articles about 1,3-bis(mesityl)imidazolium hydrogen carbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

potassium hydrogencarbonate (298-14-6) + 1,3-bis(mesityl)imidazolium chloride (141556-45-8) → 1,3-bis(mesityl)imidazolium hydrogen carbonate (1372124-93-0)

Guidance literature:

potassium hydrogencarbonate; 1,3-bis(mesityl)imidazolium chloride; at 60 ℃; for 12h;

In methanol; at 20 ℃; for 48h;

DOI:10.1021/ja3005804

Reference yield: 96.0%

carbon disulfide (75-15-0,12122-00-8) + 1,3-bis(mesityl)imidazolium hydrogen carbonate (1372124-93-0) → 1,3-bis(2,4,6-trimethylphenyl)imidazolium-2-dithiocarboxylate (917604-43-4)

Guidance literature:

In tetrahydrofuran; at 20 - 60 ℃; for 2h;

DOI:10.1021/ja3005804

Reference yield:

1,3-bis(mesityl)imidazolium hydrogen carbonate (1372124-93-0) + methyloxirane (75-56-9,16033-71-9) → 1,2-propylene cyclic carbonate (108-32-7)

Guidance literature:

With C₂₄H₁₆AlClN₂O₂; at 25 ℃; for 36h;

DOI:10.1039/d0gc00458h

upstream raw materials:

potassium hydrogencarbonate

1,3-bis(mesityl)imidazolium chloride

Downstream raw materials:

1,3-bis(2,4,6-trimethylphenyl)imidazolium-2-dithiocarboxylate

1,2-propylene cyclic carbonate

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