cyclo-<4-(asparaginyl-4-iodophenylalanylphenylalanyl-D-tryptophyl-N-ε-t-butoxycarbonyl-lysyl-O-t-butylthreonylphenylalanylamino)butanoic acid>

Base Information

Chemical Name:cyclo-<4-(asparaginyl-4-iodophenylalanylphenylalanyl-D-tryptophyl-N-ε-t-butoxycarbonyl-lysyl-O-t-butylthreonylphenylalanylamino)butanoic acid>
CAS No.:108826-78-4
Molecular Formula:C₆₅H₈₄IN₁₁O₁₂
Molecular Weight:1338.35
Hs Code.:

cyclo-<4-(asparaginyl-4-iodophenylalanylphenylalanyl-D-tryptophyl-N-ε-t-butoxycarbonyl-lysyl-O-t-butylthreonylphenylalanylamino)butanoic acid>

Synonyms:cyclo-<4-(asparaginyl-4-iodophenylalanylphenylalanyl-D-tryptophyl-N-ε-t-butoxycarbonyl-lysyl-O-t-butylthreonylphenylalanylamino)butanoic acid>

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of cyclo-<4-(asparaginyl-4-iodophenylalanylphenylalanyl-D-tryptophyl-N-ε-t-butoxycarbonyl-lysyl-O-t-butylthreonylphenylalanylamino)butanoic acid>

Chemical Property:

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Technology Process of cyclo-<4-(asparaginyl-4-iodophenylalanylphenylalanyl-D-tryptophyl-N-ε-t-butoxycarbonyl-lysyl-O-t-butylthreonylphenylalanylamino)butanoic acid>

There total 1 articles about cyclo-<4-(asparaginyl-4-iodophenylalanylphenylalanyl-D-tryptophyl-N-ε-t-butoxycarbonyl-lysyl-O-t-butylthreonylphenylalanylamino)butanoic acid> which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 31.0%

: 108826-77-3
4-(asparaginyl-4-iodophenylalanylphenylalanyl-D-tryptophyl-N-ε-t-butoxycarbonyl-lysyl-O-t-butylthreonylphenylalanylamino)butanoic acid

: 108826-78-4
cyclo-<4-(asparaginyl-4-iodophenylalanylphenylalanyl-D-tryptophyl-N-ε-t-butoxycarbonyl-lysyl-O-t-butylthreonylphenylalanylamino)butanoic acid>

Guidance literature:: With benzotriazol-1-ol; dicyclohexyl-carbodiimide; In N,N-dimethyl-formamide; at 50 ℃; for 20h;

Reference yield:

: 108826-78-4
cyclo-<4-(asparaginyl-4-iodophenylalanylphenylalanyl-D-tryptophyl-N-ε-t-butoxycarbonyl-lysyl-O-t-butylthreonylphenylalanylamino)butanoic acid>

: C₆₅H₈₄⁽³⁾HN₁₁O₁₂

Guidance literature:: With tritium; palladium on activated charcoal; rhodium on CaCO₃; In N,N-dimethyl-formamide; for 0.666667h; Ambient temperature;

Reference yield:

: 108826-78-4
cyclo-<4-(asparaginyl-4-iodophenylalanylphenylalanyl-D-tryptophyl-N-ε-t-butoxycarbonyl-lysyl-O-t-butylthreonylphenylalanylamino)butanoic acid>

: 108827-34-5
cyclo-<4-(asparaginyl-<4-(3)H>phenylalanyl-D-tryptophyl-lysylthreonylphenylalanylamino)butanoic acid>

Guidance literature:: Multi-step reaction with 2 steps

1: tritium / 10percent Pd-C, 5percent Rh-CaCO₃ / dimethylformamide / 0.67 h / Ambient temperature

2: 90percent aq. CF₃COOH / 1 h / Ambient temperature

With tritium; trifluoroacetic acid; palladium on activated charcoal; rhodium on CaCO₃; In N,N-dimethyl-formamide;