(S)-(2-((2-(1-(tert-butoxycarbonyl)-1H-indol-3-yl)ethyl)(1-phenylethyl)amino)-2-oxoethyl)dimethylsulfonium bromide

Base Information

Chemical Name:(S)-(2-((2-(1-(tert-butoxycarbonyl)-1H-indol-3-yl)ethyl)(1-phenylethyl)amino)-2-oxoethyl)dimethylsulfonium bromide
CAS No.:1431767-75-7
Molecular Formula:Br*C₂₇H₃₅N₂O₃S
Molecular Weight:547.556
Hs Code.:

Synonyms:(S)-(2-((2-(1-(tert-butoxycarbonyl)-1H-indol-3-yl)ethyl)(1-phenylethyl)amino)-2-oxoethyl)dimethylsulfonium bromide

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Chemical Property of (S)-(2-((2-(1-(tert-butoxycarbonyl)-1H-indol-3-yl)ethyl)(1-phenylethyl)amino)-2-oxoethyl)dimethylsulfonium bromide

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Technology Process of (S)-(2-((2-(1-(tert-butoxycarbonyl)-1H-indol-3-yl)ethyl)(1-phenylethyl)amino)-2-oxoethyl)dimethylsulfonium bromide

There total 5 articles about (S)-(2-((2-(1-(tert-butoxycarbonyl)-1H-indol-3-yl)ethyl)(1-phenylethyl)amino)-2-oxoethyl)dimethylsulfonium bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 75-18-3
dimethylsulfide

: 1431767-74-6
(S)-tert-butyl 3-(2-(2-bromo-N-(1-phenylethyl)acetamido)ethyl)-1H-indole-1-carboxylate

: 1431767-75-7
(S)-(2-((2-(1-(tert-butoxycarbonyl)-1H-indol-3-yl)ethyl)(1-phenylethyl)amino)-2-oxoethyl)dimethylsulfonium bromide

Guidance literature:: In dichloromethane; at 20 ℃; for 18h;
DOI:10.1016/j.tetlet.2013.03.068

Reference yield:

: 1431767-73-5
(S)-(tert-butyl) 3-(2-(1-phenylethylamino)ethyl)-1H-indole-1-carboxylate

: 1431767-75-7
(S)-(2-((2-(1-(tert-butoxycarbonyl)-1H-indol-3-yl)ethyl)(1-phenylethyl)amino)-2-oxoethyl)dimethylsulfonium bromide

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / chloroform / 1 h / 0 °C

2: dichloromethane / 18 h / 20 °C

With potassium carbonate; In dichloromethane; chloroform;
DOI:10.1016/j.tetlet.2013.03.068

Reference yield:

: 3389-21-7
3-(2-bromoethyl)-1H-indole

: 1431767-75-7
(S)-(2-((2-(1-(tert-butoxycarbonyl)-1H-indol-3-yl)ethyl)(1-phenylethyl)amino)-2-oxoethyl)dimethylsulfonium bromide

Guidance literature:: Multi-step reaction with 4 steps

1: triethylamine; dmap / dichloromethane / 12 h / 0 - 20 °C

2: potassium carbonate / acetonitrile / 4 h / Reflux

3: potassium carbonate / chloroform / 1 h / 0 °C

4: dichloromethane / 18 h / 20 °C

With dmap; potassium carbonate; triethylamine; In dichloromethane; chloroform; acetonitrile;
DOI:10.1016/j.tetlet.2013.03.068