phenylthio 2,3,4-tri-O-benzyl- 6-hydroxy-α-D-glucopyranosyl-(1→4)-2,3-di-O-benzyl-6-hydroxy-β-D-glucopyranoside

Base Information

Chemical Name:phenylthio 2,3,4-tri-O-benzyl- 6-hydroxy-α-D-glucopyranosyl-(1→4)-2,3-di-O-benzyl-6-hydroxy-β-D-glucopyranoside
CAS No.:263878-59-7
Molecular Formula:C₅₃H₅₆O₁₀S
Molecular Weight:885.088
Hs Code.:

Synonyms:phenylthio 2,3,4-tri-O-benzyl- 6-hydroxy-α-D-glucopyranosyl-(1→4)-2,3-di-O-benzyl-6-hydroxy-β-D-glucopyranoside

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Chemical Property of phenylthio 2,3,4-tri-O-benzyl- 6-hydroxy-α-D-glucopyranosyl-(1→4)-2,3-di-O-benzyl-6-hydroxy-β-D-glucopyranoside

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Technology Process of phenylthio 2,3,4-tri-O-benzyl- 6-hydroxy-α-D-glucopyranosyl-(1→4)-2,3-di-O-benzyl-6-hydroxy-β-D-glucopyranoside

There total 5 articles about phenylthio 2,3,4-tri-O-benzyl- 6-hydroxy-α-D-glucopyranosyl-(1→4)-2,3-di-O-benzyl-6-hydroxy-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: C₈₅H₉₂O₁₀SSi₂

: 263878-59-7
phenylthio 2,3,4-tri-O-benzyl- 6-hydroxy-α-D-glucopyranosyl-(1→4)-2,3-di-O-benzyl-6-hydroxy-β-D-glucopyranoside

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃;
DOI:10.1016/j.tetlet.2018.05.021

Reference yield:

: C₆₅H₈₄O₁₀SSi₂

: 263878-59-7
phenylthio 2,3,4-tri-O-benzyl- 6-hydroxy-α-D-glucopyranosyl-(1→4)-2,3-di-O-benzyl-6-hydroxy-β-D-glucopyranoside

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃; for 0.75h;
DOI:10.3987/com-99-s92

Reference yield:

: 100-39-0
benzyl bromide

: 263878-59-7
phenylthio 2,3,4-tri-O-benzyl- 6-hydroxy-α-D-glucopyranosyl-(1→4)-2,3-di-O-benzyl-6-hydroxy-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: NaH / dimethylformamide / 4 h / 20 °C

2: TBAF*3H₂O / tetrahydrofuran / 0.75 h / 20 °C

With tetrabutyl ammonium fluoride; sodium hydride; In tetrahydrofuran; N,N-dimethyl-formamide; 1: Alkylation / 2: desilylation;
DOI:10.3987/com-99-s92