(S)-Thiophosphoric acid O-(4-nitro-phenyl) ester O'-((1S,2R,3R,4S,5S,6R)-2,3,4,5,6-pentahydroxy-cyclohexyl) ester

Base Information

Chemical Name:(S)-Thiophosphoric acid O-(4-nitro-phenyl) ester O'-((1S,2R,3R,4S,5S,6R)-2,3,4,5,6-pentahydroxy-cyclohexyl) ester
CAS No.:516497-84-0
Molecular Formula:C₁₂H₁₆NO₁₀PS
Molecular Weight:397.299
Hs Code.:

Synonyms:(S)-Thiophosphoric acid O-(4-nitro-phenyl) ester O'-((1S,2R,3R,4S,5S,6R)-2,3,4,5,6-pentahydroxy-cyclohexyl) ester

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Chemical Property of (S)-Thiophosphoric acid O-(4-nitro-phenyl) ester O'-((1S,2R,3R,4S,5S,6R)-2,3,4,5,6-pentahydroxy-cyclohexyl) ester

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Technology Process of (S)-Thiophosphoric acid O-(4-nitro-phenyl) ester O'-((1S,2R,3R,4S,5S,6R)-2,3,4,5,6-pentahydroxy-cyclohexyl) ester

There total 5 articles about (S)-Thiophosphoric acid O-(4-nitro-phenyl) ester O'-((1S,2R,3R,4S,5S,6R)-2,3,4,5,6-pentahydroxy-cyclohexyl) ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 100-02-7,78813-13-5,89830-32-0
4-nitro-phenol

: 516497-84-0
(S)-Thiophosphoric acid O-(4-nitro-phenyl) ester O'-((1S,2R,3R,4S,5S,6R)-2,3,4,5,6-pentahydroxy-cyclohexyl) ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: CHCl₃ / 0 - 20 °C

2.1: sulfur / CS₂ / 12 h / 20 °C

3.1: trimethylamine / 50 °C

3.2: BF₃*Et₂O; EtSH / 1 h / 20 °C

With sulfur; trimethylamine; In carbon disulfide; chloroform;
DOI:10.1021/ja029362s

Reference yield:

: 153996-50-0
1D-1-O-2,3,4,5,6-(pentakis)methoxymethylene-myo-inositol

: 516497-84-0
(S)-Thiophosphoric acid O-(4-nitro-phenyl) ester O'-((1S,2R,3R,4S,5S,6R)-2,3,4,5,6-pentahydroxy-cyclohexyl) ester

Guidance literature:: Multi-step reaction with 4 steps

1.1: diisopropylethylamine / CHCl₃ / 6 h / -78 - 20 °C

2.1: CHCl₃ / 0 - 20 °C

3.1: sulfur / CS₂ / 12 h / 20 °C

4.1: trimethylamine / 50 °C

4.2: BF₃*Et₂O; EtSH / 1 h / 20 °C

With sulfur; N-ethyl-N,N-diisopropylamine; trimethylamine; In carbon disulfide; chloroform;
DOI:10.1021/ja029362s

Reference yield:

: Phosphorochloridous acid methyl ester (1S,2R,3R,4S,5S,6R)-2,3,4,5,6-pentakis-methoxymethoxy-cyclohexyl ester

: 516497-84-0
(S)-Thiophosphoric acid O-(4-nitro-phenyl) ester O'-((1S,2R,3R,4S,5S,6R)-2,3,4,5,6-pentahydroxy-cyclohexyl) ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: CHCl₃ / 0 - 20 °C

2.1: sulfur / CS₂ / 12 h / 20 °C

3.1: trimethylamine / 50 °C

3.2: BF₃*Et₂O; EtSH / 1 h / 20 °C

With sulfur; trimethylamine; In carbon disulfide; chloroform;
DOI:10.1021/ja029362s