1-methyl-N⁶-<3-<3-<(dimethylamino)methyl>phenoxy>propyl>-1H-1,2,4-triazole-3,5-diamine

Base Information

• Chemical Name: 1-methyl-N⁶-<3-<3-<(dimethylamino)methyl>phenoxy>propyl>-1H-1,2,4-triazole-3,5-diamine
• CAS No.: 73278-22-5
• Molecular Formula: C₁₅H₂₄N₆O
• Molecular Weight: 304.395

Synonyms:1-methyl-N⁶-<3-<3-<(dimethylamino)methyl>phenoxy>propyl>-1H-1,2,4-triazole-3,5-diamine

Chemical Property of 1-methyl-N⁶-<3-<3-<(dimethylamino)methyl>phenoxy>propyl>-1H-1,2,4-triazole-3,5-diamine

Chemical Property:

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Technology Process of 1-methyl-N⁶-<3-<3-<(dimethylamino)methyl>phenoxy>propyl>-1H-1,2,4-triazole-3,5-diamine

There total 6 articles about 1-methyl-N⁶-<3-<3-<(dimethylamino)methyl>phenoxy>propyl>-1H-1,2,4-triazole-3,5-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

N'-cyano-N-<3-<3-<(dimethylamino)methyl>phenoxy>propyl>-O-phenylisourea (84035-82-5) + methylhydrazine (60-34-4) → 1-methyl-N6-<3-<3-<(dimethylamino)methyl>phenoxy>propyl>-1H-1,2,4-triazole-3,5-diamine (73278-22-5)

Guidance literature:

In diethyl ether; 1.) 1 h; 2.) reflux, 1 h;

DOI:10.1002/jhet.5570240153

Reference yield:

N-cyano-1-methyl-2-(phenylmethylene)-hydrazinecarboximidothioic acid methyl ester + 3-(3-aminopropoxy)-N,N-dimethylbenzenemethanamine (69384-05-0) → 1-methyl-N6-<3-<3-<(dimethylamino)methyl>phenoxy>propyl>-1H-1,2,4-triazole-3,5-diamine (73278-22-5)

Guidance literature:

With hydrogenchloride; mercury; In acetone;

Reference yield:

N-Cyano-N-[3-[3-[(dimethylamino)methyl]phenoxy]propyl]carbamimidothioic acid methyl ester + methylhydrazine (60-34-4) → 1-methyl-N6-<3-<3-<(dimethylamino)methyl>phenoxy>propyl>-1H-1,2,4-triazole-3,5-diamine (73278-22-5)

Guidance literature:

In N-methyl-acetamide;

upstream raw materials:

N'-cyano-N-<3-<3-<(dimethylamino)methyl>phenoxy>propyl>-O-phenylisourea

methylhydrazine

3-(3-aminopropoxy)-N,N-dimethylbenzenemethanamine

Downstream raw materials:

N-(5-{3-[3-(dimethylamino-methyl)-phenoxy]-propylamino}-1-methyl-1H-[1,2,4]triazol-3-yl)-carbamic acid ethyl ester

N-(5-{3-[3-(dimethylamino-methyl)-phenoxy]-propylamino}-1-methyl-1H-[1,2,4]triazol-3-yl)-acetamide

(5-chloro-2-methyl-2H-[1,2,4]triazol-3-yl)-[3-(3-dimethylaminomethyl-phenoxy)-propyl]-amine

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