C₂₅H₄₂O₆Si

Base Information

Chemical Name:C₂₅H₄₂O₆Si
CAS No.:902454-62-0
Molecular Formula:C₂₅H₄₂O₆Si
Molecular Weight:466.69
Hs Code.:

C<sub>25</sub>H<sub>42</sub>O<sub>6</sub>Si

Synonyms:C₂₅H₄₂O₆Si

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Chemical Property of C₂₅H₄₂O₆Si

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Technology Process of C₂₅H₄₂O₆Si

There total 14 articles about C₂₅H₄₂O₆Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 902454-56-2
C₂₅H₄₂O₅Si

: 902454-62-0
C₂₅H₄₂O₆Si

: C₂₅H₄₂O₆Si

Guidance literature:: C₂₅H₄₂O₅Si; With potassium hexamethylsilazane; In tetrahydrofuran; toluene; at -78 ℃; for 0.5h;

With (+)-[(8,8-dichlorocamphoryl)sulfonyl]oxaziridine; In tetrahydrofuran; toluene; at -78 ℃; for 1h; Further stages. Title compound not separated from byproducts.;
DOI:10.1039/b602021f

Reference yield:

: 902454-48-2
C₁₀H₂₀O₃

: 902454-62-0
C₂₅H₄₂O₆Si

Guidance literature:: Multi-step reaction with 9 steps

1.1: NaH / tetrahydrofuran; various solvent(s) / 0.5 h / 0 °C

2.1: O₃ / CH₂Cl₂ / -78 °C

2.2: PPh₃ / CH₂Cl₂ / 1 h / -78 - 25 °C

3.1: 28.9 g / benzene / 40 h / 70 °C

4.1: 96 percent / DIBAL-H / toluene; tetrahydrofuran / 2.5 h / -78 °C

5.1: TsOH*H₂O / acetone / 3 h / 25 °C

6.1: 25.84 g / imidazole; 4-DMAP / CH₂Cl₂ / 1.5 h / 25 °C

7.1: 78 percent / NaH₂PO₄; NaClO₂; 2-methyl-2-butene / 2-methyl-propan-2-ol; H₂O / 2 h / 25 °C

8.1: 97 percent / K₂CO₃ / acetone / 16 h / 25 °C

9.1: KHMDS / tetrahydrofuran; toluene / 0.5 h / -78 °C

9.2: Davis oxaziridine / tetrahydrofuran; toluene / 1 h / -78 °C

With 1H-imidazole; dmap; sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; potassium hexamethylsilazane; sodium hydride; diisobutylaluminium hydride; potassium carbonate; toluene-4-sulfonic acid; ozone; In tetrahydrofuran; dichloromethane; water; acetone; toluene; tert-butyl alcohol; benzene; 3.1: Wittig reaction;
DOI:10.1039/b602021f

Reference yield:

: 824-94-2
p-methoxybenzyl chloride

: 902454-62-0
C₂₅H₄₂O₆Si

Guidance literature:: Multi-step reaction with 9 steps

1.1: NaH / tetrahydrofuran; various solvent(s) / 0.5 h / 0 °C

2.1: O₃ / CH₂Cl₂ / -78 °C

2.2: PPh₃ / CH₂Cl₂ / 1 h / -78 - 25 °C

3.1: 28.9 g / benzene / 40 h / 70 °C

4.1: 96 percent / DIBAL-H / toluene; tetrahydrofuran / 2.5 h / -78 °C

5.1: TsOH*H₂O / acetone / 3 h / 25 °C

6.1: 25.84 g / imidazole; 4-DMAP / CH₂Cl₂ / 1.5 h / 25 °C

7.1: 78 percent / NaH₂PO₄; NaClO₂; 2-methyl-2-butene / 2-methyl-propan-2-ol; H₂O / 2 h / 25 °C

8.1: 97 percent / K₂CO₃ / acetone / 16 h / 25 °C

9.1: KHMDS / tetrahydrofuran; toluene / 0.5 h / -78 °C

9.2: Davis oxaziridine / tetrahydrofuran; toluene / 1 h / -78 °C

With 1H-imidazole; dmap; sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; potassium hexamethylsilazane; sodium hydride; diisobutylaluminium hydride; potassium carbonate; toluene-4-sulfonic acid; ozone; In tetrahydrofuran; dichloromethane; water; acetone; toluene; tert-butyl alcohol; benzene; 3.1: Wittig reaction;
DOI:10.1039/b602021f