4-Trifluoracetylamino-1-phenyl-1,2,3,4-tetrahydro-1-naphthylessigsaeureethylester

Base Information

Chemical Name:4-Trifluoracetylamino-1-phenyl-1,2,3,4-tetrahydro-1-naphthylessigsaeureethylester
CAS No.:81124-90-5
Molecular Formula:C₂₂H₂₂F₃NO₃
Molecular Weight:405.417
Hs Code.:

Synonyms:4-Trifluoracetylamino-1-phenyl-1,2,3,4-tetrahydro-1-naphthylessigsaeureethylester

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Chemical Property of 4-Trifluoracetylamino-1-phenyl-1,2,3,4-tetrahydro-1-naphthylessigsaeureethylester

Chemical Property:

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Technology Process of 4-Trifluoracetylamino-1-phenyl-1,2,3,4-tetrahydro-1-naphthylessigsaeureethylester

There total 4 articles about 4-Trifluoracetylamino-1-phenyl-1,2,3,4-tetrahydro-1-naphthylessigsaeureethylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 38.0%

: 345307-79-1
4-Amino-1-phenyl-1,2,3,4-tetrahydro-1-naphthylessigsaeureethylester

: 407-25-0
trifluoroacetic anhydride

: 81124-90-5
4-Trifluoracetylamino-1-phenyl-1,2,3,4-tetrahydro-1-naphthylessigsaeureethylester

Guidance literature:: In diethyl ether; for 1h; Ambient temperature;
DOI:10.1002/ardp.19823150109

Reference yield:

: 81124-87-0
4-Phenyl-4-(carboxy-methyl)-1-tetralon

: 81124-90-5
4-Trifluoracetylamino-1-phenyl-1,2,3,4-tetrahydro-1-naphthylessigsaeureethylester

Guidance literature:: Multi-step reaction with 4 steps

1: 78 percent / p-toluenesulfonic acid / CHCl₃ / 8 h

2: 93 percent / H₂NOH*HCl, CH₃COONa / aq. ethanol / 2 h / Heating

3: H₂ / Ni-Raney / ethanol / 60 °C

4: 38 percent / diethyl ether / 1 h / Ambient temperature

With hydroxylamine hydrochloride; hydrogen; sodium acetate; toluene-4-sulfonic acid; Ni-Raney; In diethyl ether; ethanol; chloroform;
DOI:10.1002/ardp.19823150109

Reference yield:

: 3389-90-0
4-Hydroximino-1-phenyl-1,2,3,4-tetrahydro-1-naphthylessigsaeureethylester

: 81124-90-5
4-Trifluoracetylamino-1-phenyl-1,2,3,4-tetrahydro-1-naphthylessigsaeureethylester

Guidance literature:: Multi-step reaction with 2 steps

1: H₂ / Ni-Raney / ethanol / 60 °C

2: 38 percent / diethyl ether / 1 h / Ambient temperature

With hydrogen; Ni-Raney; In diethyl ether; ethanol;
DOI:10.1002/ardp.19823150109