diethyl 3-(p-chlorophenylhydrazono)-2-phenyl-3-phenylsulfonylpropen-1,1-dicarboxylate

Base Information

Chemical Name:diethyl 3-(p-chlorophenylhydrazono)-2-phenyl-3-phenylsulfonylpropen-1,1-dicarboxylate
CAS No.:321736-16-7
Molecular Formula:C₂₇H₂₅ClN₂O₆S
Molecular Weight:541.024
Hs Code.:

Synonyms:diethyl 3-(p-chlorophenylhydrazono)-2-phenyl-3-phenylsulfonylpropen-1,1-dicarboxylate

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Chemical Property of diethyl 3-(p-chlorophenylhydrazono)-2-phenyl-3-phenylsulfonylpropen-1,1-dicarboxylate

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Technology Process of diethyl 3-(p-chlorophenylhydrazono)-2-phenyl-3-phenylsulfonylpropen-1,1-dicarboxylate

There total 3 articles about diethyl 3-(p-chlorophenylhydrazono)-2-phenyl-3-phenylsulfonylpropen-1,1-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 106-47-8
4-chloro-aniline

: 321735-98-2
Diethyl 2-phenyl-3-(phenylsulfonyl)propene-1,1-dicarboxylate

: 321736-16-7
diethyl 3-(p-chlorophenylhydrazono)-2-phenyl-3-phenylsulfonylpropen-1,1-dicarboxylate

Guidance literature:: 4-chloro-aniline; With hydrogenchloride; sodium nitrite; at 0 - 5 ℃;

Diethyl 2-phenyl-3-(phenylsulfonyl)propene-1,1-dicarboxylate; With sodium acetate; In ethanol; water; at 20 ℃; for 3h;
DOI:10.1080/10426500008082394

Reference yield:

: 873-55-2
sodium benzenesulfonate

: 321736-16-7
diethyl 3-(p-chlorophenylhydrazono)-2-phenyl-3-phenylsulfonylpropen-1,1-dicarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1.1: 65 percent / ethanol / 3 h / Heating

2.1: conc. aq. HCl; NaNO₂ / 0 - 5 °C

2.2: 65 percent / NaOAc / ethanol; H₂O / 3 h / 20 °C

With hydrogenchloride; sodium nitrite; In ethanol;
DOI:10.1080/10426500008082394

Reference yield:

: 106352-17-4
diethyl 3-bromo-2-phenylpropene-1,1-dicarboxylate

: 321736-16-7
diethyl 3-(p-chlorophenylhydrazono)-2-phenyl-3-phenylsulfonylpropen-1,1-dicarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1.1: 65 percent / ethanol / 3 h / Heating

2.1: conc. aq. HCl; NaNO₂ / 0 - 5 °C

2.2: 65 percent / NaOAc / ethanol; H₂O / 3 h / 20 °C

With hydrogenchloride; sodium nitrite; In ethanol;
DOI:10.1080/10426500008082394