(1S,2S,3a⁽¹⁾S,12bS)-1-hydroxy-2,3a⁽¹⁾,4,5,7,12b-hexahydro-1H-[1,3]dioxolo[4,5-j]pyrrolo[3,2,1-de]phenanthridin-1,2-diyl dibenzoate

Base Information

• Chemical Name: (1S,2S,3a⁽¹⁾S,12bS)-1-hydroxy-2,3a⁽¹⁾,4,5,7,12b-hexahydro-1H-[1,3]dioxolo[4,5-j]pyrrolo[3,2,1-de]phenanthridin-1,2-diyl dibenzoate
• CAS No.: 1350717-32-6
• Molecular Formula: C₃₀H₂₅NO₆
• Molecular Weight: 495.532

Synonyms:(1S,2S,3a⁽¹⁾S,12bS)-1-hydroxy-2,3a⁽¹⁾,4,5,7,12b-hexahydro-1H-[1,3]dioxolo[4,5-j]pyrrolo[3,2,1-de]phenanthridin-1,2-diyl dibenzoate

Chemical Property of (1S,2S,3a⁽¹⁾S,12bS)-1-hydroxy-2,3a⁽¹⁾,4,5,7,12b-hexahydro-1H-[1,3]dioxolo[4,5-j]pyrrolo[3,2,1-de]phenanthridin-1,2-diyl dibenzoate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (1S,2S,3a⁽¹⁾S,12bS)-1-hydroxy-2,3a⁽¹⁾,4,5,7,12b-hexahydro-1H-[1,3]dioxolo[4,5-j]pyrrolo[3,2,1-de]phenanthridin-1,2-diyl dibenzoate

There total 3 articles about (1S,2S,3a⁽¹⁾S,12bS)-1-hydroxy-2,3a⁽¹⁾,4,5,7,12b-hexahydro-1H-[1,3]dioxolo[4,5-j]pyrrolo[3,2,1-de]phenanthridin-1,2-diyl dibenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

benzoyl chloride (98-88-4) + lycorine (476-28-8,6835-91-2,19312-40-4,66816-51-1) → (1S,2S,3a(1)S,12bS)-1-hydroxy-2,3a(1),4,5,7,12b-hexahydro-1H-[1,3]dioxolo[4,5-j]pyrrolo[3,2,1-de]phenanthridin-1,2-diyl dibenzoate (1350717-32-6)

Guidance literature:

With pyridine; dmap; at 40 ℃; for 5h; Inert atmosphere;

DOI:10.1016/j.bmc.2011.09.051

Reference yield: 47.0%

benzoyl chloride (98-88-4) + lycorine (476-28-8,6835-91-2,19312-40-4,66816-51-1) → (1S,2S,3a(1)S,12bS)-1-hydroxy-2,3a(1),4,5,7,12b-hexahydro-1H-[1,3]dioxolo[4,5-j]pyrrolo[3,2,1-de]phenanthridin-2-yl benzoate (1350717-33-7) + (1S,2S,3a(1)S,12bS)-1-hydroxy-2,3a(1),4,5,7,12b-hexahydro-1H-[1,3]dioxolo[4,5-j]pyrrolo[3,2,1-de]phenanthridin-1,2-diyl dibenzoate (1350717-32-6)

Guidance literature:

With pyridine; dmap; at 20 ℃; for 48h;

DOI:10.1111/j.1747-0285.2012.01333.x

Reference yield: 47.0%

→ (1S,2S,3a(1)S,12bS)-1-hydroxy-2,3a(1),4,5,7,12b-hexahydro-1H-[1,3]dioxolo[4,5-j]pyrrolo[3,2,1-de]phenanthridin-1,2-diyl dibenzoate (1350717-32-6)

Guidance literature:

With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; for 24h; Reflux;

upstream raw materials:

benzoyl chloride

lycorine

Downstream raw materials:

(1S,2S,3a⁽¹⁾S,12bS)-2-hydroxy-2,3a⁽¹⁾,4,5,7,12b-hexahydro-1H-[1,3]dioxolo[4,5-j]pyrrolo[3,2,1-de]phenanthridin-1-yl benzoate

(1S,2S,3a⁽¹⁾S,12bS)-1-hydroxy-2,3a⁽¹⁾,4,5,7,12b-hexahydro-1H-[1,3]dioxolo[4,5-j]pyrrolo[3,2,1-de]phenanthridin-2-yl benzoate

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 1350717-32-6 (1S,2S,3a⁽¹⁾S,12bS)-1-hydroxy-2,3a⁽¹⁾,4,5,7,12b-hexahydro-1H-[1,3]dioxolo[4,5-j]pyrrolo[3,2,1-de]phenanthridin-1,2-diyl dibenzoate

Send

Send

Metric Ton KG G Pound L ML

Send

Send