C₂₂H₃₃N₃O₈

Base Information

Chemical Name:C₂₂H₃₃N₃O₈
CAS No.:1421971-11-0
Molecular Formula:C₂₂H₃₃N₃O₈
Molecular Weight:467.519
Hs Code.:

C<sub>22</sub>H<sub>33</sub>N<sub>3</sub>O<sub>8</sub>

Synonyms:C₂₂H₃₃N₃O₈

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Chemical Property of C₂₂H₃₃N₃O₈

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Technology Process of C₂₂H₃₃N₃O₈

There total 4 articles about C₂₂H₃₃N₃O₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 16642-79-8
3-(4-nitrophenyl)propionic acid

: 1421971-10-9
C₁₃H₂₅ClN₂O₄

: 1421971-11-0
C₂₂H₃₃N₃O₈

Guidance literature:: 3-(4-nitrophenyl)propionic acid; With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 2h;

C₁₃H₂₅ClN₂O₄; In N,N-dimethyl-formamide; at -10 - 20 ℃; for 12.5h;

Reference yield:

: 626-95-9
1,4-Pentanediol

: 1421971-11-0
C₂₂H₃₃N₃O₈

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium azide; triphenylphosphine / tetrachloromethane; N,N-dimethyl-formamide / 90 °C

1.2: 0.17 h / 20 °C

2.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 1.5 h / -10 - 0 °C

3.1: triethylamine / dichloromethane / 0.5 h / 0 °C

4.1: potassium carbonate / N,N-dimethyl-formamide / 2 h / 20 °C

4.2: 12.5 h / -10 - 20 °C

With sodium azide; potassium carbonate; triethylamine; N-ethyl-N,N-diisopropylamine; triphenylphosphine; In tetrachloromethane; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 591-77-5
1-methyl-1,4-butanediamine

: 1421971-11-0
C₂₂H₃₃N₃O₈

Guidance literature:: Multi-step reaction with 3 steps

1.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 1.5 h / -10 - 0 °C

2.1: triethylamine / dichloromethane / 0.5 h / 0 °C

3.1: potassium carbonate / N,N-dimethyl-formamide / 2 h / 20 °C

3.2: 12.5 h / -10 - 20 °C

With potassium carbonate; triethylamine; N-ethyl-N,N-diisopropylamine; In dichloromethane; N,N-dimethyl-formamide;