2,2'-[(1-methylethylidene)bis(4,1-phenyleneoxyethane-2,1-diyloxyethane-2,1-diyloxy)]bis[ethanol]

Base Information

Chemical Name:2,2'-[(1-methylethylidene)bis(4,1-phenyleneoxyethane-2,1-diyloxyethane-2,1-diyloxy)]bis[ethanol]
CAS No.:114539-46-7
Molecular Formula:C₂₇H₄₀O₈
Molecular Weight:492.61
Hs Code.:

Synonyms:2,2'-[(1-methylethylidene)bis(4,1-phenyleneoxyethane-2,1-diyloxyethane-2,1-diyloxy)]bis[ethanol]

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Chemical Property of 2,2'-[(1-methylethylidene)bis(4,1-phenyleneoxyethane-2,1-diyloxyethane-2,1-diyloxy)]bis[ethanol]

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Technology Process of 2,2'-[(1-methylethylidene)bis(4,1-phenyleneoxyethane-2,1-diyloxyethane-2,1-diyloxy)]bis[ethanol]

There total 1 articles about 2,2'-[(1-methylethylidene)bis(4,1-phenyleneoxyethane-2,1-diyloxyethane-2,1-diyloxy)]bis[ethanol] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 80-05-7
BPA

: 62573-16-4
2-[2-(2-iodoethoxy)ethoxy]ethanol

: 114539-46-7,99280-30-5
2,2'-[(1-methylethylidene)bis(4,1-phenyleneoxyethane-2,1-diyloxyethane-2,1-diyloxy)]bis[ethanol]

Guidance literature:: With caesium carbonate; In N,N-dimethyl-formamide; at 60 ℃; for 24h;
DOI:10.1002/hlca.200390345

Reference yield: 93.0%

: 124-63-0
methanesulfonyl chloride

: 114539-46-7,99280-30-5
2,2'-[(1-methylethylidene)bis(4,1-phenyleneoxyethane-2,1-diyloxyethane-2,1-diyloxy)]bis[ethanol]

: 671756-16-4
2,2'-[(1-methylethylidene)bis(4,1-phenyleneoxyethane-2,1-diyloxyethane-2,1-diyloxy)]bis[ethanol] dimethanesulfonate

Guidance literature:: With triethylamine; In dichloromethane; at -5 - 4 ℃;
DOI:10.1002/hlca.200390345

Reference yield:

: 114539-46-7,99280-30-5
2,2'-[(1-methylethylidene)bis(4,1-phenyleneoxyethane-2,1-diyloxyethane-2,1-diyloxy)]bis[ethanol]

: 671756-19-7
C₂₇H₃₈Br₂O₆

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / Et₃N / CH₂Cl₂ / -5 - 4 °C

2: 92 percent / LiBr / acetone / 4 h / Heating

With triethylamine; lithium bromide; In dichloromethane; acetone;
DOI:10.1002/hlca.200390345