C₂₉H₄₂O₅Si

Base Information

Chemical Name:C₂₉H₄₂O₅Si
CAS No.:1032879-87-0
Molecular Formula:C₂₉H₄₂O₅Si
Molecular Weight:498.735
Hs Code.:

C<sub>29</sub>H<sub>42</sub>O<sub>5</sub>Si

Synonyms:C₂₉H₄₂O₅Si

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Chemical Property of C₂₉H₄₂O₅Si

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Technology Process of C₂₉H₄₂O₅Si

There total 8 articles about C₂₉H₄₂O₅Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 1032879-85-8
C₂₇H₃₈O₅Si

: 1826-67-1
vinyl magnesium bromide

: 1032879-87-0
C₂₉H₄₂O₅Si

Guidance literature:: C₂₇H₃₈O₅Si; vinyl magnesium bromide; In diethyl ether; at -78 ℃; for 3h;

With sodium hydrogencarbonate; In diethyl ether; water;
DOI:10.1021/ol8008057

Reference yield:

: 101331-92-4
4-O-(tert-butyldiphenylsilyl)-2,3-O-isopropylidene-L-threose

: 1032879-87-0
C₂₉H₄₂O₅Si

Guidance literature:: Multi-step reaction with 5 steps

1.1: (-)-B-methoxydiisopinocamphenylborane / diethyl ether / 1 h / 0 - 20 °C

1.2: 3 h / -78 °C

2.1: sodium hydride / tetrahydrofuran / 1 h / -10 - 20 °C

2.2: 12 h / 20 °C

3.1: 9-bora-bicyclo[3.3.1]nonane / tetrahydrofuran / 5 h / 0 - 20 °C

3.2: 2 h / Reflux

4.1: dimethyl sulfoxide; triethylamine; sulfur trioxide pyridine complex / dichloromethane / 2 h / -10 °C

5.1: diethyl ether / 3 h / -78 °C

With (-)-B-methoxydiisopinocamphenylborane; sulfur trioxide pyridine complex; sodium hydride; dimethyl sulfoxide; triethylamine; 9-bora-bicyclo[3.3.1]nonane; In tetrahydrofuran; diethyl ether; dichloromethane;
DOI:10.3987/COM-12-S(N)54

Reference yield:

: 1032879-81-4
C₂₇H₃₈O₄Si

: 1032879-87-0
C₂₉H₄₂O₅Si

Guidance literature:: Multi-step reaction with 3 steps

1.1: 9-bora-bicyclo[3.3.1]nonane / tetrahydrofuran / 5 h / 0 - 20 °C

1.2: 2 h / Reflux

2.1: dimethyl sulfoxide; triethylamine; sulfur trioxide pyridine complex / dichloromethane / 2 h / -10 °C

3.1: diethyl ether / 3 h / -78 °C

With sulfur trioxide pyridine complex; dimethyl sulfoxide; triethylamine; 9-bora-bicyclo[3.3.1]nonane; In tetrahydrofuran; diethyl ether; dichloromethane;
DOI:10.3987/COM-12-S(N)54