1,3-acetonedicarboxylic acid diphenyl ester

Base Information

Chemical Name:1,3-acetonedicarboxylic acid diphenyl ester
CAS No.:41395-84-0
Molecular Formula:C₁₇H₁₄O₅
Molecular Weight:298.295
Hs Code.:

Synonyms:1,3-acetonedicarboxylic acid diphenyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,3-acetonedicarboxylic acid diphenyl ester

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Technology Process of 1,3-acetonedicarboxylic acid diphenyl ester

There total 3 articles about 1,3-acetonedicarboxylic acid diphenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 35756-54-8
malonic acid monophenyl ester

: 41395-84-0
1,3-acetonedicarboxylic acid diphenyl ester

Guidance literature:: With O-(N-succinimidyl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; for 0.5h;
DOI:10.1016/j.tetlet.2003.08.014

Reference yield:

: 108-95-2,27073-41-2
phenol

: 41395-84-0
1,3-acetonedicarboxylic acid diphenyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / toluene / Heating

2: 82 percent / TSTU; N,N-diisopropylethylamine / dimethylformamide / 0.5 h

With O-(N-succinimidyl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; toluene;
DOI:10.1016/j.tetlet.2003.08.014