rac-(β,β-²H₂)styrene oxide

Base Information

Chemical Name:rac-(β,β-²H₂)styrene oxide
CAS No.:66255-92-3
Molecular Formula:C₈H₈O
Molecular Weight:122.135
Hs Code.:

rac-(β,β-<sup>2</sup>H<sub>2</sub>)styrene oxide

Synonyms:rac-(β,β-²H₂)styrene oxide

Suppliers and Price of rac-(β,β-²H₂)styrene oxide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of rac-(β,β-²H₂)styrene oxide

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of rac-(β,β-²H₂)styrene oxide

There total 9 articles about rac-(β,β-²H₂)styrene oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 934-85-0
styrene-d2

: 66255-92-3
rac-(β,β-²H₂)styrene oxide

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In tetrachloromethane; at 20 ℃; for 4h; Cooling with ice;
DOI:10.1002/hlca.201200444

Reference yield: 84.0%

: 87372-49-4
<ω-(2)H2>-ω-bromoacetophenone

: 66255-92-3
rac-(β,β-²H₂)styrene oxide

Guidance literature:: <ω-(2)H2>-ω-bromoacetophenone; With sodium tetrahydroborate; In methanol; at 0 - 20 ℃; for 3h; Schlenk technique; Inert atmosphere;

With potassium carbonate; In methanol; for 15h;
DOI:10.1021/acs.joc.8b01374

Reference yield:

: 17537-31-4
Acetophenone-methyl-d3

: 66255-92-3
rac-(β,β-²H₂)styrene oxide

Guidance literature:: Multi-step reaction with 3 steps

1.1: lithium aluminium tetrahydride / tetrahydrofuran / 2 h / 20 °C / Inert atmosphere; Cooling with ice

1.2: Inert atmosphere; Cooling with ice

2.1: potassium hydrogensulfate; 4-tert-Butylcatechol / 180 °C / 45 Torr

3.1: 3-chloro-benzenecarboperoxoic acid / tetrachloromethane / 4 h / 20 °C / Cooling with ice

With potassium hydrogensulfate; lithium aluminium tetrahydride; 4-tert-Butylcatechol; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; tetrachloromethane;
DOI:10.1002/hlca.201200444