[4-((2S,3R,4R,5S,6R)-3,4-Dihydroxy-6-hydroxymethyl-5-methoxy-tetrahydro-pyran-2-yloxy)-phenyl]-carbamic acid isopropyl ester

Base Information

Chemical Name:[4-((2S,3R,4R,5S,6R)-3,4-Dihydroxy-6-hydroxymethyl-5-methoxy-tetrahydro-pyran-2-yloxy)-phenyl]-carbamic acid isopropyl ester
CAS No.:102992-50-7
Molecular Formula:C₁₇H₂₅NO₈
Molecular Weight:371.387
Hs Code.:

Synonyms:[4-((2S,3R,4R,5S,6R)-3,4-Dihydroxy-6-hydroxymethyl-5-methoxy-tetrahydro-pyran-2-yloxy)-phenyl]-carbamic acid isopropyl ester

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Chemical Property of [4-((2S,3R,4R,5S,6R)-3,4-Dihydroxy-6-hydroxymethyl-5-methoxy-tetrahydro-pyran-2-yloxy)-phenyl]-carbamic acid isopropyl ester

Chemical Property:

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MSDS Files:: SDS file from LookChem

Useful:

Technology Process of [4-((2S,3R,4R,5S,6R)-3,4-Dihydroxy-6-hydroxymethyl-5-methoxy-tetrahydro-pyran-2-yloxy)-phenyl]-carbamic acid isopropyl ester

There total 4 articles about [4-((2S,3R,4R,5S,6R)-3,4-Dihydroxy-6-hydroxymethyl-5-methoxy-tetrahydro-pyran-2-yloxy)-phenyl]-carbamic acid isopropyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 3295-92-9
N-methyl N-phenyl carbamate d'isopropyle

: 5327-53-7
4 hydroxy Probham

: 122-42-9
carbamic acid, phenyl-, 1-methylethyl ester

: 102992-50-7
[4-((2S,3R,4R,5S,6R)-3,4-Dihydroxy-6-hydroxymethyl-5-methoxy-tetrahydro-pyran-2-yloxy)-phenyl]-carbamic acid isopropyl ester

Guidance literature:: With Beauveria sulfurescens ATCC 7159; at 28 ℃; for 48h;
DOI:10.1016/0040-4020(86)80008-4

Reference yield: 22.0%

: 122-42-9
carbamic acid, phenyl-, 1-methylethyl ester

: 5327-53-7
4 hydroxy Probham

: 102992-50-7
[4-((2S,3R,4R,5S,6R)-3,4-Dihydroxy-6-hydroxymethyl-5-methoxy-tetrahydro-pyran-2-yloxy)-phenyl]-carbamic acid isopropyl ester

Guidance literature:: With Beauveria sulfurescens ATCC 7159; at 28 ℃; for 48h;
DOI:10.1016/0040-4020(86)80008-4

Reference yield:

: 122-42-9
carbamic acid, phenyl-, 1-methylethyl ester

: 102992-50-7
[4-((2S,3R,4R,5S,6R)-3,4-Dihydroxy-6-hydroxymethyl-5-methoxy-tetrahydro-pyran-2-yloxy)-phenyl]-carbamic acid isopropyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 97 percent / potassium hydroxyde / dimethylsulfoxide / 0.5 h

2: 39 percent / Beauveria sulfurescens ATCC 7159 / 48 h / 28 °C

With potassium hydroxide; Beauveria sulfurescens ATCC 7159; In dimethyl sulfoxide;
DOI:10.1016/0040-4020(86)80008-4