bis{ω-[4-(4-cyanophenyl)phenoxy]hexyl} 4,4'-diamino-biphenyl-2,2'-dicarboxylate

Base Information

Chemical Name:bis{ω-[4-(4-cyanophenyl)phenoxy]hexyl} 4,4'-diamino-biphenyl-2,2'-dicarboxylate
CAS No.:351195-57-8
Molecular Formula:C₅₂H₅₀N₄O₆
Molecular Weight:826.992
Hs Code.:

Synonyms:bis{ω-[4-(4-cyanophenyl)phenoxy]hexyl} 4,4'-diamino-biphenyl-2,2'-dicarboxylate

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Chemical Property of bis{ω-[4-(4-cyanophenyl)phenoxy]hexyl} 4,4'-diamino-biphenyl-2,2'-dicarboxylate

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Technology Process of bis{ω-[4-(4-cyanophenyl)phenoxy]hexyl} 4,4'-diamino-biphenyl-2,2'-dicarboxylate

There total 6 articles about bis{ω-[4-(4-cyanophenyl)phenoxy]hexyl} 4,4'-diamino-biphenyl-2,2'-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 351195-58-9
bis{ω-[4-(4-cyanophenyl)phenoxy]hexyl}4,4'-dinitro-biphenyl-2,2'-dicarboxylate

: 351195-57-8
bis{ω-[4-(4-cyanophenyl)phenoxy]hexyl} 4,4'-diamino-biphenyl-2,2'-dicarboxylate

Guidance literature:: With tin(ll) chloride; In ethanol; for 4h; Heating;
DOI:10.1021/ja0042682

Reference yield:

: 629-11-8
1,6-hexanediol

: 351195-57-8
bis{ω-[4-(4-cyanophenyl)phenoxy]hexyl} 4,4'-diamino-biphenyl-2,2'-dicarboxylate

Guidance literature:: Multi-step reaction with 4 steps

1: 42 percent / HBr; H₂SO₄ / H₂O / 2 h / Heating

2: 92 percent / K₂CO₃ / acetone / 24 h / Heating

3: 76 percent / DCC; DMAP / CH₂Cl₂ / 24 h / 20 °C

4: 75 percent / SnCl₂ / ethanol / 4 h / Heating

With dmap; sulfuric acid; hydrogen bromide; potassium carbonate; dicyclohexyl-carbodiimide; tin(ll) chloride; In ethanol; dichloromethane; water; acetone;
DOI:10.1021/ja0042682

Reference yield:

: 4286-55-9
1-bromo-6-hexanol

: 351195-57-8
bis{ω-[4-(4-cyanophenyl)phenoxy]hexyl} 4,4'-diamino-biphenyl-2,2'-dicarboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: 92 percent / K₂CO₃ / acetone / 24 h / Heating

2: 76 percent / DCC; DMAP / CH₂Cl₂ / 24 h / 20 °C

3: 75 percent / SnCl₂ / ethanol / 4 h / Heating

With dmap; potassium carbonate; dicyclohexyl-carbodiimide; tin(ll) chloride; In ethanol; dichloromethane; acetone;
DOI:10.1021/ja0042682