Technology Process of C21H34N2O6S
There total 7 articles about C21H34N2O6S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
trifluoroacetic acid;
In
dichloromethane;
at 20 ℃;
for 2h;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 20 °C
2.1: water; acetic acid / tetrahydrofuran / 3 h / 20 °C
3.1: pyridinium chlorochromate / dichloromethane / 20 °C
4.1: sodium chlorite; sodium dihydrogenphosphate / water; acetonitrile / 2 h / 0 - 20 °C
4.3: pH 2
5.1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 20 °C
6.1: trifluoroacetic acid / dichloromethane / 2 h / 20 °C
With
dmap; sodium chlorite; sodium dihydrogenphosphate; water; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; pyridinium chlorochromate; trifluoroacetic acid;
In
tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: pyridinium chlorochromate / dichloromethane / 20 °C
2.1: sodium chlorite; sodium dihydrogenphosphate / water; acetonitrile / 2 h / 0 - 20 °C
2.3: pH 2
3.1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 20 °C
4.1: trifluoroacetic acid / dichloromethane / 2 h / 20 °C
With
dmap; sodium chlorite; sodium dihydrogenphosphate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; pyridinium chlorochromate; trifluoroacetic acid;
In
dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;