[4-(1-butyl-1H-[1,2,3]triazol-4-yl)phenyl](4-trifluoromethylphenyl)diazene

Base Information

Chemical Name:[4-(1-butyl-1H-[1,2,3]triazol-4-yl)phenyl](4-trifluoromethylphenyl)diazene
CAS No.:1622350-29-1
Molecular Formula:C₁₉H₁₈F₃N₅
Molecular Weight:373.381
Hs Code.:

Synonyms:[4-(1-butyl-1H-[1,2,3]triazol-4-yl)phenyl](4-trifluoromethylphenyl)diazene

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Chemical Property of [4-(1-butyl-1H-[1,2,3]triazol-4-yl)phenyl](4-trifluoromethylphenyl)diazene

Chemical Property:

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Technology Process of [4-(1-butyl-1H-[1,2,3]triazol-4-yl)phenyl](4-trifluoromethylphenyl)diazene

There total 5 articles about [4-(1-butyl-1H-[1,2,3]triazol-4-yl)phenyl](4-trifluoromethylphenyl)diazene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.2%

: 7332-00-5
n-butylazide

: 1429060-64-9
(4-ethynylphenyl)(4-trifluoromethylphenyl)diazene

: 1622350-29-1
[4-(1-butyl-1H-[1,2,3]triazol-4-yl)phenyl](4-trifluoromethylphenyl)diazene

Guidance literature:: With copper(l) iodide; In N,N-dimethyl-formamide; at 100 ℃;
DOI:10.1080/15421406.2013.827842

Reference yield:

: 455-14-1
4-trifluoromethylphenylamine

: 1622350-29-1
[4-(1-butyl-1H-[1,2,3]triazol-4-yl)phenyl](4-trifluoromethylphenyl)diazene

Guidance literature:: Multi-step reaction with 5 steps

1: Oxone / dichloromethane / 15 h / 20 °C / Inert atmosphere

2: acetic acid / 15 h / 20 °C

3: triethylamine; copper(l) iodide; triphenylphosphine; bis-triphenylphosphine-palladium(II) chloride / tetrahydrofuran / 10 h / 30 °C / Inert atmosphere

4: potassium carbonate / tetrahydrofuran; methanol / 20 °C

5: copper(l) iodide / N,N-dimethyl-formamide / 100 °C

With bis-triphenylphosphine-palladium(II) chloride; Oxone; copper(l) iodide; potassium carbonate; acetic acid; triethylamine; triphenylphosphine; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; 5: |Huisgen Cycloaddition;
DOI:10.1080/15421406.2013.827842

Reference yield:

: 1641560-83-9
C₁₈H₁₇F₃N₂Si

: 1622350-29-1
[4-(1-butyl-1H-[1,2,3]triazol-4-yl)phenyl](4-trifluoromethylphenyl)diazene

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / tetrahydrofuran; methanol / 20 °C

2: copper(l) iodide / N,N-dimethyl-formamide / 100 °C

With copper(l) iodide; potassium carbonate; In tetrahydrofuran; methanol; N,N-dimethyl-formamide; 2: |Huisgen Cycloaddition;
DOI:10.1080/15421406.2013.827842