3-(triphenylphosphonium bromide-methyl)-5-isobutoxy-N-(thiazol-2-yl)benzamide

Base Information

Chemical Name:3-(triphenylphosphonium bromide-methyl)-5-isobutoxy-N-(thiazol-2-yl)benzamide
CAS No.:1282520-83-5
Molecular Formula:Br*C₃₃H₃₂N₂O₂PS
Molecular Weight:631.573
Hs Code.:

Synonyms:3-(triphenylphosphonium bromide-methyl)-5-isobutoxy-N-(thiazol-2-yl)benzamide

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Chemical Property of 3-(triphenylphosphonium bromide-methyl)-5-isobutoxy-N-(thiazol-2-yl)benzamide

Chemical Property:

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Technology Process of 3-(triphenylphosphonium bromide-methyl)-5-isobutoxy-N-(thiazol-2-yl)benzamide

There total 5 articles about 3-(triphenylphosphonium bromide-methyl)-5-isobutoxy-N-(thiazol-2-yl)benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.5%

: 1282520-87-9
3-bromomethyl-5-isobutoxy-N-(thiazol-2-yl)-benzamide

: 603-35-0
triphenylphosphine

: 1282520-83-5
3-(triphenylphosphonium bromide-methyl)-5-isobutoxy-N-(thiazol-2-yl)benzamide

Guidance literature:: In benzene; at 100 ℃; for 6h;

Reference yield:

: 1185753-91-6
dimethyl 5-(isobutyloxy)isophthalate

: 1282520-83-5
3-(triphenylphosphonium bromide-methyl)-5-isobutoxy-N-(thiazol-2-yl)benzamide

Guidance literature:: Multi-step reaction with 5 steps

1: potassium hydroxide; methanol / tetrahydrofuran / 10 h / 100 °C

2: dicyclohexyl-carbodiimide / dichloromethane / 12 h / 20 °C

3: lithium borohydride; ethanol / tetrahydrofuran / 48 h / 0 - 20 °C

4: tribromo phosphate / tetrahydrofuran / 12 h / 0 - 20 °C

5: benzene / 6 h / 100 °C

With methanol; lithium borohydride; ethanol; tribromo phosphate; dicyclohexyl-carbodiimide; potassium hydroxide; In tetrahydrofuran; dichloromethane; benzene;

Reference yield:

: 1282520-84-6
3-isobutoxy-5-(methoxycarbonyl)benzoic acid

: 1282520-83-5
3-(triphenylphosphonium bromide-methyl)-5-isobutoxy-N-(thiazol-2-yl)benzamide

Guidance literature:: Multi-step reaction with 4 steps

1: dicyclohexyl-carbodiimide / dichloromethane / 12 h / 20 °C

2: lithium borohydride; ethanol / tetrahydrofuran / 48 h / 0 - 20 °C

3: tribromide phosphate / tetrahydrofuran / 12 h / 0 - 20 °C

4: benzene / 6 h / 100 °C

With lithium borohydride; ethanol; tribromide phosphate; dicyclohexyl-carbodiimide; In tetrahydrofuran; dichloromethane; benzene;