(2R,3S,4S)-1-benzyl-3,4-bis-(tert-butyldimethylsilyloxy)-2-triphenylmethoxymethylpyrrolidine

Base Information

Chemical Name:(2R,3S,4S)-1-benzyl-3,4-bis-(tert-butyldimethylsilyloxy)-2-triphenylmethoxymethylpyrrolidine
CAS No.:443127-35-3
Molecular Formula:C₄₃H₅₉NO₃Si₂
Molecular Weight:694.117
Hs Code.:

Synonyms:(2R,3S,4S)-1-benzyl-3,4-bis-(tert-butyldimethylsilyloxy)-2-triphenylmethoxymethylpyrrolidine

Suppliers and Price of (2R,3S,4S)-1-benzyl-3,4-bis-(tert-butyldimethylsilyloxy)-2-triphenylmethoxymethylpyrrolidine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2R,3S,4S)-1-benzyl-3,4-bis-(tert-butyldimethylsilyloxy)-2-triphenylmethoxymethylpyrrolidine

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Technology Process of (2R,3S,4S)-1-benzyl-3,4-bis-(tert-butyldimethylsilyloxy)-2-triphenylmethoxymethylpyrrolidine

There total 1 articles about (2R,3S,4S)-1-benzyl-3,4-bis-(tert-butyldimethylsilyloxy)-2-triphenylmethoxymethylpyrrolidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 62-53-3
aniline

: 443127-33-1
2,3-bis-O-tert-butyldimethylsilyl-1,4-bis-O-methanesulfonyl-5-O-triphenylmethyl-L-arabinitol

: 443127-35-3
(2R,3S,4S)-1-benzyl-3,4-bis-(tert-butyldimethylsilyloxy)-2-triphenylmethoxymethylpyrrolidine

Guidance literature:: at 85 ℃; for 60h;
DOI:10.1021/jo025538x

Reference yield:

: 443127-35-3
(2R,3S,4S)-1-benzyl-3,4-bis-(tert-butyldimethylsilyloxy)-2-triphenylmethoxymethylpyrrolidine

: (2R,3S,4S)-3,4-Bis-(tert-butyl-dimethyl-silanyloxy)-2-trityloxymethyl-pyrrolidine

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethanol; at 20 ℃; for 8h; atmospheric pressure;
DOI:10.1021/jo025538x

Reference yield:

: 443127-35-3
(2R,3S,4S)-1-benzyl-3,4-bis-(tert-butyldimethylsilyloxy)-2-triphenylmethoxymethylpyrrolidine

: (2R,3S,4S)-3,4-bis-(tert-butyldimethylsilyloxy)-1-fluorenylmethoxycarbonyl-2-triphenylmethoxy-methylpyrrolidine

Guidance literature:: Multi-step reaction with 2 steps

1: H₂ / Pd/C / ethanol / 8 h / 20 °C / atmospheric pressure

2: Et₃N / toluene / 16 h / 20 °C

With hydrogen; triethylamine; palladium on activated charcoal; In ethanol; toluene;
DOI:10.1021/jo025538x