rac-chloro((RS)-o-phenylenebis(methylphenylphosphine))((RR,SS)-o-phenylenebis(methylphenylphosphine))nickel(II)hexafluorophosphate

Base Information

Chemical Name:rac-chloro((RS)-o-phenylenebis(methylphenylphosphine))((RR,SS)-o-phenylenebis(methylphenylphosphine))nickel(II)hexafluorophosphate
CAS No.:77059-67-7
Molecular Formula:C₄₀H₄₀ClNiP₄*F₆P
Molecular Weight:883.76
Hs Code.:

Synonyms:rac-chloro((RS)-o-phenylenebis(methylphenylphosphine))((RR,SS)-o-phenylenebis(methylphenylphosphine))nickel(II)hexafluorophosphate

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Chemical Property of rac-chloro((RS)-o-phenylenebis(methylphenylphosphine))((RR,SS)-o-phenylenebis(methylphenylphosphine))nickel(II)hexafluorophosphate

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Technology Process of rac-chloro((RS)-o-phenylenebis(methylphenylphosphine))((RR,SS)-o-phenylenebis(methylphenylphosphine))nickel(II)hexafluorophosphate

There total 1 articles about rac-chloro((RS)-o-phenylenebis(methylphenylphosphine))((RR,SS)-o-phenylenebis(methylphenylphosphine))nickel(II)hexafluorophosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: ammonium hexafluorophosphate

: 122331-49-1
(R*,R*)-(+/-)-1,2-phenylenebis(methylphenylphosphine)

: 87760-26-7,77029-28-8
{T-4-(R(*),S(*))}-dicarbonyl{1,2-phenylenebis(methylphenylphosphine)}nickel⁽⁰⁾

: 77059-67-7
rac-chloro((RS)-o-phenylenebis(methylphenylphosphine))((RR,SS)-o-phenylenebis(methylphenylphosphine))nickel(II)hexafluorophosphate

Guidance literature:: With sulfuryl dichloride; In ethanol; dichloromethane; water; byproducts: CO, SO2; dicarbinyl dissolved in dichloromethane and soln. treated with SO2Cl2 in dichloromethane at 0°C under N2 atm., after 20 min (RR,SS)-diphos added, solvent removed and residue dissolved in ethanol, NH4PF6 in water added; ppt. washed and dried and recrystd. from dichloromethane by addn. diethyl ether; elem. anal.;