α-Phenylisocinchomeronic acid

Base Information

• Chemical Name: α-Phenylisocinchomeronic acid
• CAS No.: 107393-00-0
• Molecular Formula: C₁₃H₉NO₄
• Molecular Weight: 243.219
• Mol file: 107393-00-0.mol

Synonyms:α-Phenylisocinchomeronic acid

Chemical Property of α-Phenylisocinchomeronic acid

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of α-Phenylisocinchomeronic acid

There total 3 articles about α-Phenylisocinchomeronic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 24.0%

3,6-dimethyl-2-phenylpyridine (27068-69-5) → α-Phenylisocinchomeronic acid (107393-00-0)

Guidance literature:

With potassium permanganate; In water; at 100 ℃; for 8h;

DOI:10.1007/BF00519533

Reference yield:

bromobenzene (108-86-1,52753-63-6) → α-Phenylisocinchomeronic acid (107393-00-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 21 percent / 1) Mg / 1) Ether, 2) reflux, 4 h.

2: 24 percent / Potassium permanganate / H₂O / 8 h / 100 °C

With potassium permanganate; magnesium; In water;

DOI:10.1007/BF00519533

Reference yield:

2,5-dimethylpyridine (589-93-5) → α-Phenylisocinchomeronic acid (107393-00-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 21 percent / 1) Mg / 1) Ether, 2) reflux, 4 h.

2: 24 percent / Potassium permanganate / H₂O / 8 h / 100 °C

With potassium permanganate; magnesium; In water;

DOI:10.1007/BF00519533

upstream raw materials:

3,6-dimethyl-2-phenylpyridine

bromobenzene

2,5-dimethylpyridine

Downstream raw materials:

α-Phenylisocinchomeronic acid dimethyl ester

α-Phenylisocinchomeronic acid dichloride

α-Phenylisocinchomeronic acid dimorpholide