3,6-Dimethyl-2-phenylpyridine

Base Information

Chemical Name:3,6-Dimethyl-2-phenylpyridine
CAS No.:27068-69-5
Molecular Formula:C13H13N
Molecular Weight:183.253
Hs Code.:
DSSTox Substance ID:DTXSID501308339
Nikkaji Number:J1.014.867G

Synonyms:3,6-dimethyl-2-phenylpyridine;SCHEMBL11733981;3,6-dimethyl-2-phenyl-pyridine;DTXSID501308339;27068-69-5

Suppliers and Price of 3,6-Dimethyl-2-phenylpyridine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3,6-Dimethyl-2-phenylpyridine

Chemical Property:

XLogP3:3.3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:1
Exact Mass:183.104799419
Heavy Atom Count:14
Complexity:172

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=C(N=C(C=C1)C)C2=CC=CC=C2

Technology Process of 3,6-Dimethyl-2-phenylpyridine

There total 16 articles about 3,6-Dimethyl-2-phenylpyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 4-methyl-4-(3-oxobutyl)-3-phenylisoxazol-5(4H)-one

: 27068-69-5
3,6-dimethyl-2-phenylpyridine

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; hydrogen; In 1,4-dioxane; at 22 ℃; under 760.051 Torr; regioselective reaction;
DOI:10.1021/acs.joc.5b01065

Reference yield: 72.0%

: 2867-59-6
2-aminobutanol

: 93-54-9
1-Phenyl-1-propanol

: 27068-69-5
3,6-dimethyl-2-phenylpyridine

Guidance literature:: With C₁₇H₁₁Cl₂N₃O₃Ru; potassium tert-butylate; In toluene; at 110 ℃; for 6h;
DOI:10.1021/acs.organomet.8b00359

Reference yield: 46.0%

: 926308-17-0
((1S,2S)-2-methyl-3-oxo-1-phenylpropyl)carbamic acid tert-butyl ester

: 1439-36-7
1-triphenylphosphoranylidene-2-propanone

: 27068-69-5
3,6-dimethyl-2-phenylpyridine

Guidance literature:: ((1S,2S)-2-methyl-3-oxo-1-phenylpropyl)carbamic acid tert-butyl ester; 1-triphenylphosphoranylidene-2-propanone; In ethyl acetate; at 80 ℃; for 12h; Inert atmosphere;

With tetrachlorosilane; In ethyl acetate; at 40 ℃; for 4h; Further stages; Inert atmosphere;