2,4-dibromo-3,6-dimethoxybenzyl chloride

Base Information

Chemical Name:2,4-dibromo-3,6-dimethoxybenzyl chloride
CAS No.:120185-74-2
Molecular Formula:C₉H₉Br₂ClO₂
Molecular Weight:344.43
Hs Code.:

Synonyms:2,4-dibromo-3,6-dimethoxybenzyl chloride

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Chemical Property of 2,4-dibromo-3,6-dimethoxybenzyl chloride

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Technology Process of 2,4-dibromo-3,6-dimethoxybenzyl chloride

There total 5 articles about 2,4-dibromo-3,6-dimethoxybenzyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 74076-59-8
2,6-dibromo-1,4-dimethoxybenzene

: 120185-74-2
2,4-dibromo-3,6-dimethoxybenzyl chloride

Guidance literature:: With hydrogenchloride; at 100 ℃;
DOI:10.1016/S0040-4039(00)95396-6

Reference yield:

: 13670-73-0
3,5-dibromo-4-methoxyphenol

: 120185-74-2
2,4-dibromo-3,6-dimethoxybenzyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / K₂CO₃ / acetone / Heating

2: 85 percent / HCl / 100 °C

With hydrogenchloride; potassium carbonate; In acetone;
DOI:10.1016/S0040-4039(00)95396-6

Reference yield:

: 51699-89-9
1,3-dibromo-2-methoxy-5-methylbenzene

: 120185-74-2
2,4-dibromo-3,6-dimethoxybenzyl chloride

Guidance literature:: Multi-step reaction with 5 steps

1: CrO₃, sulphuric acid / acetic acid / 1 h / 0 °C

2: methanol, K₂CO₃ / 2 h

3: 60 percent / m-chloroperbenzoic acid, H₂SO₄ / CH₂Cl₂ / 1) 2h, 2) H₂O, 6 h RT

4: K₂CO₃ / acetone / 2 h / Heating

5: 35percent HCl / 4 h / Heating

With chromium(VI) oxide; hydrogenchloride; methanol; sulfuric acid; potassium carbonate; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; acetic acid; acetone;
DOI:10.1016/S0040-4020(01)86201-3