ethyl 4-(2-(4-(2,3,4-trimethoxybenzyl)piperazin-1-yl)ethoxy)-3-aminobenzoate

Base Information

Chemical Name:ethyl 4-(2-(4-(2,3,4-trimethoxybenzyl)piperazin-1-yl)ethoxy)-3-aminobenzoate
CAS No.:1235166-28-5
Molecular Formula:C₂₅H₃₅N₃O₆
Molecular Weight:473.569
Hs Code.:

Synonyms:ethyl 4-(2-(4-(2,3,4-trimethoxybenzyl)piperazin-1-yl)ethoxy)-3-aminobenzoate

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Chemical Property of ethyl 4-(2-(4-(2,3,4-trimethoxybenzyl)piperazin-1-yl)ethoxy)-3-aminobenzoate

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Technology Process of ethyl 4-(2-(4-(2,3,4-trimethoxybenzyl)piperazin-1-yl)ethoxy)-3-aminobenzoate

There total 3 articles about ethyl 4-(2-(4-(2,3,4-trimethoxybenzyl)piperazin-1-yl)ethoxy)-3-aminobenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 1235166-22-9
ethyl 4-(2-(4-(2,3,4-trimethoxybenzyl)piperazin-1-yl)ethoxy)-3-nitrobenzoate

: 1235166-28-5
ethyl 4-(2-(4-(2,3,4-trimethoxybenzyl)piperazin-1-yl)ethoxy)-3-aminobenzoate

Guidance literature:: With hydrogenchloride; iron; In ethanol; water; for 1h; Reflux;
DOI:10.1016/j.ejmech.2011.06.011

Reference yield:

: 19013-10-6
ethyl 4-hydroxy-3-nitrobenzoate

: 1235166-28-5
ethyl 4-(2-(4-(2,3,4-trimethoxybenzyl)piperazin-1-yl)ethoxy)-3-aminobenzoate

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium carbonate / acetonitrile / 4 h / Reflux

2.1: potassium hydroxide / water / pH Ca_. 11

2.2: 4 h / Reflux

3.1: hydrogenchloride; iron / ethanol; water / 1 h / Reflux

With hydrogenchloride; iron; potassium carbonate; potassium hydroxide; In ethanol; water; acetonitrile;
DOI:10.1016/j.ejmech.2011.06.011

Reference yield:

: 386213-23-6
ethyl 4-(2-bromoethoxy)-3-nitrobenzoate

: 1235166-28-5
ethyl 4-(2-(4-(2,3,4-trimethoxybenzyl)piperazin-1-yl)ethoxy)-3-aminobenzoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium hydroxide / water / pH Ca_. 11

1.2: 4 h / Reflux

2.1: hydrogenchloride; iron / ethanol; water / 1 h / Reflux

With hydrogenchloride; iron; potassium hydroxide; In ethanol; water;
DOI:10.1016/j.ejmech.2011.06.011