Decane, 1,1,1,2,3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10-eicosafluoro-10-iodo-2-(trifluoromethyl)-

Base Information

Chemical Name:Decane, 1,1,1,2,3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10-eicosafluoro-10-iodo-2-(trifluoromethyl)-
CAS No.:677-93-0
Molecular Formula:C11F23 I
Molecular Weight:695.989
Hs Code.:
European Community (EC) Number:211-645-4
DSSTox Substance ID:DTXSID5060984
Nikkaji Number:J205.979G
Wikidata:Q81989254
Mol file:677-93-0.mol

Synonyms:677-93-0;Decane, 1,1,1,2,3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10-eicosafluoro-10-iodo-2-(trifluoromethyl)-;PERFLUOROISOUNDECYL IODIDE;1,1,1,2,3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10-icosafluoro-10-iodo-2-(trifluoromethyl)decane;Icosafluoro-10-iodo-2-(trifluoromethyl)decane;Decane, eicosafluoro-1-iodo-9-(trifluoromethyl)-;EINECS 211-645-4;PERFLUOROISOUNDECYLIODIDE;SCHEMBL3919976;DTXSID5060984;Perfluoro-1-iodo-9-methyldecane;C11F23I;C11-F23-I;MFCD00153245;1,1,1,2,3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10-Icosafluoro-10-iodo-2-trifluoromethyldecane

Suppliers and Price of Decane, 1,1,1,2,3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10-eicosafluoro-10-iodo-2-(trifluoromethyl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
PERFLUOROISOUNDECYL IODIDE 95.00%
10G
$ 1222.28

American Custom Chemicals Corporation
PERFLUOROISOUNDECYL IODIDE 95.00%
5G
$ 870.65

Total 14 raw suppliers

Chemical Property of Decane, 1,1,1,2,3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10-eicosafluoro-10-iodo-2-(trifluoromethyl)-

Chemical Property:

Vapor Pressure:0.175mmHg at 25°C
Boiling Point:80°C 5mm
Flash Point:101.4°C
PSA：0.00000
Density:1.961g/cm³
LogP:8.29420
XLogP3:8.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:23
Rotatable Bond Count:8
Exact Mass:695.86775
Heavy Atom Count:35
Complexity:768

Purity/Quality:

98%min ^*data from raw suppliers

PERFLUOROISOUNDECYL IODIDE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:T
Statements: 36/37/38
Safety Statements: 26-36/37/39

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C(C(C(C(C(C(C(C(C(F)(F)I)(F)F)(F)F)(F)F)(F)F)(F)F)(F)F)(F)F)(C(F)(F)F)(C(F)(F)F)F

Technology Process of Decane, 1,1,1,2,3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10-eicosafluoro-10-iodo-2-(trifluoromethyl)-

There total 1 articles about Decane, 1,1,1,2,3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10-eicosafluoro-10-iodo-2-(trifluoromethyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 116-14-3,82785-14-6
polytetrafluoroethylene

: 677-69-0
perfluoroisopropyl iodide

: 3486-08-6
1-iodoperfluoroisoheptane

: 865-77-0
7-methylperfluorooctyl iodide

: 677-93-0
9-methylperfluorodecyl iodide

Guidance literature:: With 2,2'-azobis(isobutyronitrile); at 78 ℃; for 18h; Further Variations:; Temperatures; Product distribution;
DOI:10.1016/j.jfluchem.2006.01.002

Reference yield:

: 1745-81-9
o-Allylphenol

: 677-93-0
9-methylperfluorodecyl iodide

: 2-(4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,12,13,13,13-eicosafluoro-12-trifluoromethyl-tridecyl)-phenol

Guidance literature:: o-Allylphenol; 9-methylperfluorodecyl iodide; With tetrakis(triphenylphosphine) palladium⁽⁰⁾; In hexane; at 25 ℃; for 36h;

With lithium aluminium tetrahydride; In diethyl ether; for 2h; Heating;
DOI:10.1021/ja036213g

Reference yield:

: 677-93-0
9-methylperfluorodecyl iodide

: 4-bromo-2-(4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,12,13,13,13-eicosafluoro-12-trifluoromethyl-tridecyl)-phenol

Guidance literature:: Multi-step reaction with 2 steps

1.1: (Ph₃P)4Pd / hexane / 36 h / 25 °C

1.2: LiAlH₄ / diethyl ether / 2 h / Heating

2.1: HBr; DMSO; AcOH / 0.5 h / 5 - 10 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; hydrogen bromide; acetic acid; dimethyl sulfoxide; In hexane;
DOI:10.1021/ja036213g