trifluoromethanesulfonic acid 3-(1,1-dimethylheptyl)-5-methoxyphenyl ester

Base Information

Chemical Name:trifluoromethanesulfonic acid 3-(1,1-dimethylheptyl)-5-methoxyphenyl ester
CAS No.:866398-19-8
Molecular Formula:C₁₇H₂₅F₃O₄S
Molecular Weight:382.444
Hs Code.:

Synonyms:trifluoromethanesulfonic acid 3-(1,1-dimethylheptyl)-5-methoxyphenyl ester

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Chemical Property of trifluoromethanesulfonic acid 3-(1,1-dimethylheptyl)-5-methoxyphenyl ester

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Technology Process of trifluoromethanesulfonic acid 3-(1,1-dimethylheptyl)-5-methoxyphenyl ester

There total 6 articles about trifluoromethanesulfonic acid 3-(1,1-dimethylheptyl)-5-methoxyphenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 358-23-6
trifluoromethylsulfonic anhydride

: 87613-50-1
3-(1,1-dimethylheptyl)-5-methoxyphenol

: 866398-19-8
trifluoromethanesulfonic acid 3-(1,1-dimethylheptyl)-5-methoxyphenyl ester

Guidance literature:: With 2,4,6-trimethyl-pyridine; In dichloromethane; at 0 ℃; for 24h;
DOI:10.1021/ol051570c

Reference yield:

: 866398-16-5
trifluoromethanesulfonic acid 4-(1,1-dimethylheptyl)-2,6-dimethoxyphenyl ester

: 866398-19-8
trifluoromethanesulfonic acid 3-(1,1-dimethylheptyl)-5-methoxyphenyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 82 percent / H₂; Et₃N / Pd/C / methanol / 192 h / 20 °C / atmospheric pressure

2: 68 percent / 1-propanethiol; NaH / dimethylformamide / 20 h / 120 °C

3: 87 percent / 2,4,6-collidine / CH₂Cl₂ / 24 h / 0 °C

With 2,4,6-trimethyl-pyridine; 1-thiopropane; hydrogen; sodium hydride; triethylamine; palladium on activated charcoal; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ol051570c

Reference yield:

: 91-10-1
1,3-dimethoxy-2-hydroxy-benzene

: 866398-19-8
trifluoromethanesulfonic acid 3-(1,1-dimethylheptyl)-5-methoxyphenyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: MsOH / 50 °C

2: 80 percent / 2,4,6-collidine / CH₂Cl₂ / 24 h / 0 °C

3: 82 percent / H₂; Et₃N / Pd/C / methanol / 192 h / 20 °C / atmospheric pressure

4: 68 percent / 1-propanethiol; NaH / dimethylformamide / 20 h / 120 °C

5: 87 percent / 2,4,6-collidine / CH₂Cl₂ / 24 h / 0 °C

With 2,4,6-trimethyl-pyridine; methanesulfonic acid; 1-thiopropane; hydrogen; sodium hydride; triethylamine; palladium on activated charcoal; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ol051570c