(R)-N-α-(tert-butoxycarbonyl)-N-methoxy-O-(methoxymethyl)-N,N-α-dimethyltyrosinamide

Base Information

Chemical Name:(R)-N-α-(tert-butoxycarbonyl)-N-methoxy-O-(methoxymethyl)-N,N-α-dimethyltyrosinamide
CAS No.:1093169-43-7
Molecular Formula:C₁₉H₃₀N₂O₆
Molecular Weight:382.457
Hs Code.:

Synonyms:(R)-N-α-(tert-butoxycarbonyl)-N-methoxy-O-(methoxymethyl)-N,N-α-dimethyltyrosinamide

Suppliers and Price of (R)-N-α-(tert-butoxycarbonyl)-N-methoxy-O-(methoxymethyl)-N,N-α-dimethyltyrosinamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (R)-N-α-(tert-butoxycarbonyl)-N-methoxy-O-(methoxymethyl)-N,N-α-dimethyltyrosinamide

Chemical Property:

Purity/Quality:

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Technology Process of (R)-N-α-(tert-butoxycarbonyl)-N-methoxy-O-(methoxymethyl)-N,N-α-dimethyltyrosinamide

There total 1 articles about (R)-N-α-(tert-butoxycarbonyl)-N-methoxy-O-(methoxymethyl)-N,N-α-dimethyltyrosinamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 1093169-42-6
(R)-N-α-(tert-butoxycarbonyl)-N-methoxy-O-(methoxymethyl)-N-methyltyrosinamide

: 74-88-4
methyl iodide

: 1093169-43-7
(R)-N-α-(tert-butoxycarbonyl)-N-methoxy-O-(methoxymethyl)-N,N-α-dimethyltyrosinamide

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; at -20 ℃;
DOI:10.1016/j.tetlet.2008.09.141

Reference yield: 90.0%

: 1093169-43-7
(R)-N-α-(tert-butoxycarbonyl)-N-methoxy-O-(methoxymethyl)-N,N-α-dimethyltyrosinamide

: 78878-05-4
1-iodo-3-(tert-butyldimethylsilyloxy)propane

: 1159215-36-7
tert-butyl (R)-[5-(tert-butyldimethylsilyloxy)-1-[4-(methoxymethoxy)benzyl]-2-oxopentyl]methylcarbamate

Guidance literature:: 1-iodo-3-(tert-butyldimethylsilyloxy)propane; With n-butyllithium; In diethyl ether; pentane; at -78 ℃; for 0.5h; Inert atmosphere;

(R)-N-α-(tert-butoxycarbonyl)-N-methoxy-O-(methoxymethyl)-N,N-α-dimethyltyrosinamide; In diethyl ether; pentane; at -78 - 20 ℃; Inert atmosphere;
DOI:10.1016/j.tet.2009.03.003

Reference yield:

: 1093169-43-7
(R)-N-α-(tert-butoxycarbonyl)-N-methoxy-O-(methoxymethyl)-N,N-α-dimethyltyrosinamide

: 1093169-28-8
C₁₇H₂₅NO₅

Guidance literature:: With diisobutylaluminium hydride; In diethyl ether; at 0 ℃; optical yield given as %ee;
DOI:10.1016/j.tetlet.2008.09.141