6-[3-(1-{2-[2-(2-azidoethoxy)ethoxy]ethyl}-1H-[1,2,3]triazol-4-yl)-4-(tetrahydropyran-2-yloxy)phenyl]-7-butyl-5-methyl-5H-pyrrolo[2,3-b]pyrazine

Base Information

Chemical Name:6-[3-(1-{2-[2-(2-azidoethoxy)ethoxy]ethyl}-1H-[1,2,3]triazol-4-yl)-4-(tetrahydropyran-2-yloxy)phenyl]-7-butyl-5-methyl-5H-pyrrolo[2,3-b]pyrazine
CAS No.:1187336-62-4
Molecular Formula:C₃₀H₃₉N₉O₄
Molecular Weight:589.698
Hs Code.:

Synonyms:6-[3-(1-{2-[2-(2-azidoethoxy)ethoxy]ethyl}-1H-[1,2,3]triazol-4-yl)-4-(tetrahydropyran-2-yloxy)phenyl]-7-butyl-5-methyl-5H-pyrrolo[2,3-b]pyrazine

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Chemical Property of 6-[3-(1-{2-[2-(2-azidoethoxy)ethoxy]ethyl}-1H-[1,2,3]triazol-4-yl)-4-(tetrahydropyran-2-yloxy)phenyl]-7-butyl-5-methyl-5H-pyrrolo[2,3-b]pyrazine

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Technology Process of 6-[3-(1-{2-[2-(2-azidoethoxy)ethoxy]ethyl}-1H-[1,2,3]triazol-4-yl)-4-(tetrahydropyran-2-yloxy)phenyl]-7-butyl-5-methyl-5H-pyrrolo[2,3-b]pyrazine

There total 1 articles about 6-[3-(1-{2-[2-(2-azidoethoxy)ethoxy]ethyl}-1H-[1,2,3]triazol-4-yl)-4-(tetrahydropyran-2-yloxy)phenyl]-7-butyl-5-methyl-5H-pyrrolo[2,3-b]pyrazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1123659-50-6
6-[3-(1-{2-[2-(2-azidoethoxy)ethoxy]ethyl}-1H-[1,2,3]triazol-4-yl)-4-(tetrahydropyran-2-yloxy)phenyl]-7-butyl-5H-pyrrolo[2,3-b]pyrazine

: 74-88-4
methyl iodide

: 1187336-62-4
6-[3-(1-{2-[2-(2-azidoethoxy)ethoxy]ethyl}-1H-[1,2,3]triazol-4-yl)-4-(tetrahydropyran-2-yloxy)phenyl]-7-butyl-5-methyl-5H-pyrrolo[2,3-b]pyrazine

Guidance literature:: 6-[3-(1-{2-[2-(2-azidoethoxy)ethoxy]ethyl}-1H-[1,2,3]triazol-4-yl)-4-(tetrahydropyran-2-yloxy)phenyl]-7-butyl-5H-pyrrolo[2,3-b]pyrazine; With caesium carbonate; In N,N-dimethyl-formamide; at 0 ℃; for 0.5h; Inert atmosphere;

methyl iodide; In N,N-dimethyl-formamide; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1016/j.bmc.2009.06.024

Reference yield: 83.0%

: 1187336-62-4
6-[3-(1-{2-[2-(2-azidoethoxy)ethoxy]ethyl}-1H-[1,2,3]triazol-4-yl)-4-(tetrahydropyran-2-yloxy)phenyl]-7-butyl-5-methyl-5H-pyrrolo[2,3-b]pyrazine

: 1187336-77-1
C₂₅H₃₁N₉O₃

Guidance literature:: 6-[3-(1-{2-[2-(2-azidoethoxy)ethoxy]ethyl}-1H-[1,2,3]triazol-4-yl)-4-(tetrahydropyran-2-yloxy)phenyl]-7-butyl-5-methyl-5H-pyrrolo[2,3-b]pyrazine; With methanol; toluene-4-sulfonic acid; at 20 ℃; for 2h; Inert atmosphere;

With potassium carbonate; In methanol; water;
DOI:10.1016/j.bmc.2009.06.024