1,3,3a,6a-tetrahydro-5-phenyl-4H-cyclopentafuran-4-one

Base Information

Chemical Name:1,3,3a,6a-tetrahydro-5-phenyl-4H-cyclopentafuran-4-one
CAS No.:122422-20-2
Molecular Formula:C₁₃H₁₂O₂
Molecular Weight:200.237
Hs Code.:

1,3,3a,6a-tetrahydro-5-phenyl-4H-cyclopenta<c>furan-4-one

Synonyms:1,3,3a,6a-tetrahydro-5-phenyl-4H-cyclopentafuran-4-one

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Chemical Property of 1,3,3a,6a-tetrahydro-5-phenyl-4H-cyclopentafuran-4-one

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Technology Process of 1,3,3a,6a-tetrahydro-5-phenyl-4H-cyclopentafuran-4-one

There total 9 articles about 1,3,3a,6a-tetrahydro-5-phenyl-4H-cyclopentafuran-4-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 1708-29-8
2,5-dihydrofuran

: 122422-20-2
1,3,3a,6a-tetrahydro-5-phenyl-4H-cyclopentafuran-4-one

Guidance literature:: With triethylamine; In toluene; for 1.75h; Ultrasound;

Reference yield: 69.0%

: 1708-29-8
2,5-dihydrofuran

: 122422-20-2
1,3,3a,6a-tetrahydro-5-phenyl-4H-cyclopentafuran-4-one

Guidance literature:: With phenylacetylene hexacarbonyldicobalt; Tributylphosphine oxide; In hexane; at 69 ℃; for 36h; Product distribution; reaction of various hexacarbonyl dicobalt complexes with various alkenes; effect of temperature, of solvents, of reaction time, of added phosphine-oxides, effect of ultrasound irradiation;
DOI:10.1016/0022-328X(88)87050-5

Reference yield: 45.0%

: 1708-29-8
2,5-dihydrofuran

: 122474-08-2
Co₂(CO)5(HC₂Ph)(PBu₃)

: 122422-20-2
1,3,3a,6a-tetrahydro-5-phenyl-4H-cyclopentafuran-4-one

Guidance literature:: In toluene; (N2); reflux the mixt. for 36 h;; filtration; evapn. of soln.; chromy. of residue (alumina column, CHCl3); solvent removal; elem. anal.;
DOI:10.1016/0022-328X(88)87050-5