4-{6-[(E)-(4-{(E)-[4-(dimethylamino)phenyl]diazenyl)phenyl)-diazenyl]-2,3-dihydro-1H-perimidin-2-yl}-phenol

Base Information

Chemical Name:4-{6-[(E)-(4-{(E)-[4-(dimethylamino)phenyl]diazenyl)phenyl)-diazenyl]-2,3-dihydro-1H-perimidin-2-yl}-phenol
CAS No.:765303-90-0
Molecular Formula:C₃₁H₂₇N₇O
Molecular Weight:513.602
Hs Code.:

Synonyms:4-{6-[(E)-(4-{(E)-[4-(dimethylamino)phenyl]diazenyl)phenyl)-diazenyl]-2,3-dihydro-1H-perimidin-2-yl}-phenol

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Chemical Property of 4-{6-[(E)-(4-{(E)-[4-(dimethylamino)phenyl]diazenyl)phenyl)-diazenyl]-2,3-dihydro-1H-perimidin-2-yl}-phenol

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Technology Process of 4-{6-[(E)-(4-{(E)-[4-(dimethylamino)phenyl]diazenyl)phenyl)-diazenyl]-2,3-dihydro-1H-perimidin-2-yl}-phenol

There total 1 articles about 4-{6-[(E)-(4-{(E)-[4-(dimethylamino)phenyl]diazenyl)phenyl)-diazenyl]-2,3-dihydro-1H-perimidin-2-yl}-phenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 539-17-3,70735-04-5
4-amino-4'-dimethylaminoazobenzene

: 123-08-0,65581-83-1
4-hydroxy-benzaldehyde

: 479-27-6
naphthalene-1,8-diamine

: 765303-90-0
4-{6-[(E)-(4-{(E)-[4-(dimethylamino)phenyl]diazenyl)phenyl)-diazenyl]-2,3-dihydro-1H-perimidin-2-yl}-phenol

Guidance literature:: 4-amino-4'-dimethylaminoazobenzene; With hydrogenchloride; sodium nitrite; In DMF (N,N-dimethyl-formamide); water; at 0 ℃; for 2h; Heating / reflux;

4-hydroxy-benzaldehyde; naphthalene-1,8-diamine; In DMF (N,N-dimethyl-formamide); ethanol; water; at 0 - 10 ℃; for 0.5h;

With potassium acetate; In DMF (N,N-dimethyl-formamide); ethanol; water; at 0 ℃; for 1h;

Reference yield: 96.0%

: 765303-90-0
4-{6-[(E)-(4-{(E)-[4-(dimethylamino)phenyl]diazenyl)phenyl)-diazenyl]-2,3-dihydro-1H-perimidin-2-yl}-phenol

: 83883-26-5
4-{[6-(acryloyloxy)hexyl]oxy}benzoic acid

: 765303-88-6
4-{6-((E)-(4-{(E)-[4-(dimethylamino)phenyl]diazenyl}phenyl)-diazenyl]-2,3-dihydro-1H-perimidin-2-yl}phenyl 4-{[6-(acryloyloxy)hexyl]oxy)-benzoate

Guidance literature:: 4-{[6-(acryloyloxy)hexyl]oxy}benzoic acid; With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 0 ℃; for 1.5h;

4-{6-[(E)-(4-{(E)-[4-(dimethylamino)phenyl]diazenyl)phenyl)-diazenyl]-2,3-dihydro-1H-perimidin-2-yl}-phenol; In dichloromethane; at 20 ℃; for 3h;