2(5H)-Furanone,4-[(3E,7E)-10-[(1S)-2,2-dimethyl-6-methylenecyclohexyl]-4,8-dimethyl-3,7-decadien-1-yl]-

Base Information

Chemical Name:2(5H)-Furanone,4-[(3E,7E)-10-[(1S)-2,2-dimethyl-6-methylenecyclohexyl]-4,8-dimethyl-3,7-decadien-1-yl]-
CAS No.:145398-68-1
Molecular Formula:C25H38 O2
Molecular Weight:370.576
Hs Code.:

Synonyms:2(5H)-Furanone,4-[(3E,7E)-10-[(1S)-2,2-dimethyl-6-methylenecyclohexyl]-4,8-dimethyl-3,7-decadienyl]-(9CI); 2(5H)-Furanone,4-[10-(2,2-dimethyl-6-methylenecyclohexyl)-4,8-dimethyl-3,7-decadienyl]-,[S-(E,E)]-; Luffarin P

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Chemical Property of 2(5H)-Furanone,4-[(3E,7E)-10-[(1S)-2,2-dimethyl-6-methylenecyclohexyl]-4,8-dimethyl-3,7-decadien-1-yl]-

Chemical Property:

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Hazard Codes:

MSDS Files:: SDS file from LookChem

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Technology Process of 2(5H)-Furanone,4-[(3E,7E)-10-[(1S)-2,2-dimethyl-6-methylenecyclohexyl]-4,8-dimethyl-3,7-decadien-1-yl]-

There total 12 articles about 2(5H)-Furanone,4-[(3E,7E)-10-[(1S)-2,2-dimethyl-6-methylenecyclohexyl]-4,8-dimethyl-3,7-decadien-1-yl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 12.0%

: (S)-2,2-dimethyl-6-methylene-1-[3'-(1''-phenyl-1''H-tetrazole-5''-sulfonyl)butyl]cyclohexane

: (3E)-3-(6-formyl-4-mehtylhex-3-enyl) but-2-en-4-olide

: C₂₅H₃₈O₂

: 145398-68-1
luffarin-P

Guidance literature:: (S)-2,2-dimethyl-6-methylene-1-[3'-(1''-phenyl-1''H-tetrazole-5''-sulfonyl)butyl]cyclohexane; With potassium hexamethylsilazane; In tetrahydrofuran; toluene; at -30 ℃; for 1h;

(3E)-3-(6-formyl-4-mehtylhex-3-enyl) but-2-en-4-olide; In tetrahydrofuran; toluene;
DOI:10.1016/j.molcatb.2015.11.019

Reference yield:

: 472-19-5,4352-33-4
(2,2-dimethyl-6-methylenecyclohexyl)methanol

: C₂₅H₃₈O₂

: 145398-68-1
luffarin-P

Guidance literature:: Multi-step reaction with 8 steps

1.1: polymer supported Candida antarctica lipase B / di-isopropyl ether / 15 h / 25 °C / Resolution of racemate; Enzymatic reaction

2.1: pyridine / 0 - 20 °C

3.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 6 h / 90 °C

4.1: dihydrogen peroxide / ethanol; water / 0 - 20 °C

5.1: n-butyllithium / tetrahydrofuran; hexane / 0 - 20 °C

5.2: 12 h / 0 °C

6.1: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran; toluene / 2 h / 0 °C

7.1: dihydrogen peroxide / ethanol; water / 0 - 20 °C

8.1: potassium hexamethylsilazane / tetrahydrofuran; toluene / 1 h / -30 °C

With pyridine; n-butyllithium; dihydrogen peroxide; potassium hexamethylsilazane; sodium hydride; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; ethanol; hexane; di-isopropyl ether; water; N,N-dimethyl-formamide; toluene; mineral oil; 6.1: |Mitsunobu Displacement / 8.1: |Julia Olefin Synthesis / 8.2: |Julia Olefin Synthesis;
DOI:10.1016/j.molcatb.2015.11.019

Reference yield:

: 502763-33-9
(S)-(-)-2,2-dimethyl-6-methylene-1-[1'-(phenylthio)methyl]cyclohexane

: C₂₅H₃₈O₂

: 145398-68-1
luffarin-P

Guidance literature:: Multi-step reaction with 5 steps

1.1: dihydrogen peroxide / ethanol; water / 0 - 20 °C

2.1: n-butyllithium / tetrahydrofuran; hexane / 0 - 20 °C

2.2: 12 h / 0 °C

3.1: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran; toluene / 2 h / 0 °C

4.1: dihydrogen peroxide / ethanol; water / 0 - 20 °C

5.1: potassium hexamethylsilazane / tetrahydrofuran; toluene / 1 h / -30 °C

With n-butyllithium; dihydrogen peroxide; potassium hexamethylsilazane; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; ethanol; hexane; water; toluene; 3.1: |Mitsunobu Displacement / 5.1: |Julia Olefin Synthesis / 5.2: |Julia Olefin Synthesis;
DOI:10.1016/j.molcatb.2015.11.019