3-[2-(2-azido-acetylamino)-4-chloro-phenyl]-3-oxo-N-phenyl-propionamide

Base Information

• Chemical Name: 3-[2-(2-azido-acetylamino)-4-chloro-phenyl]-3-oxo-N-phenyl-propionamide
• CAS No.: 350238-07-2
• Molecular Formula: C₁₇H₁₄ClN₅O₃
• Molecular Weight: 371.783

Synonyms:3-[2-(2-azido-acetylamino)-4-chloro-phenyl]-3-oxo-N-phenyl-propionamide

Chemical Property of 3-[2-(2-azido-acetylamino)-4-chloro-phenyl]-3-oxo-N-phenyl-propionamide

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Technology Process of 3-[2-(2-azido-acetylamino)-4-chloro-phenyl]-3-oxo-N-phenyl-propionamide

There total 5 articles about 3-[2-(2-azido-acetylamino)-4-chloro-phenyl]-3-oxo-N-phenyl-propionamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-chloro-2-nitro-benzoic acid (6280-88-2) → 3-[2-(2-azido-acetylamino)-4-chloro-phenyl]-3-oxo-N-phenyl-propionamide (350238-07-2)

Guidance literature:

Multi-step reaction with 6 steps

1: SOCl₂

2: MgCl₂; Et₃N / acetonitrile

3: 85 percent / xylene / Heating

4: 97 percent / Fe; CaCl₂ / ethanol

5: 45 percent / pyridine / diethyl ether

6: 50 percent / NaN₃ / dimethylsulfoxide

With pyridine; thionyl chloride; sodium azide; iron; triethylamine; calcium chloride; magnesium chloride; In diethyl ether; ethanol; dimethyl sulfoxide; acetonitrile; xylene;

DOI:10.1016/S0040-4039(01)00402-6

Reference yield:

4-chloro-2-nitro-benzoyl chloride (41995-04-4) → 3-[2-(2-azido-acetylamino)-4-chloro-phenyl]-3-oxo-N-phenyl-propionamide (350238-07-2)

Guidance literature:

Multi-step reaction with 5 steps

1: MgCl₂; Et₃N / acetonitrile

2: 85 percent / xylene / Heating

3: 97 percent / Fe; CaCl₂ / ethanol

4: 45 percent / pyridine / diethyl ether

5: 50 percent / NaN₃ / dimethylsulfoxide

With pyridine; sodium azide; iron; triethylamine; calcium chloride; magnesium chloride; In diethyl ether; ethanol; dimethyl sulfoxide; acetonitrile; xylene;

DOI:10.1016/S0040-4039(01)00402-6

Reference yield:

ethyl 4-chloro-2-nitrobenzoylacetate (220101-42-8) → 3-[2-(2-azido-acetylamino)-4-chloro-phenyl]-3-oxo-N-phenyl-propionamide (350238-07-2)

Guidance literature:

Multi-step reaction with 4 steps

1: 85 percent / xylene / Heating

2: 97 percent / Fe; CaCl₂ / ethanol

3: 45 percent / pyridine / diethyl ether

4: 50 percent / NaN₃ / dimethylsulfoxide

With pyridine; sodium azide; iron; calcium chloride; In diethyl ether; ethanol; dimethyl sulfoxide; xylene;

DOI:10.1016/S0040-4039(01)00402-6

upstream raw materials:

4-chloro-2-nitro-benzoic acid

4-chloro-2-nitro-benzoyl chloride

ethyl 4-chloro-2-nitrobenzoylacetate

3-(2-amino-4-chloro-phenyl)-3-oxo-N-phenyl-propionamide

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