1-(1-(2,6-dimethylphenylimino)-2,2-dimethylpropyl)-3-(2,4,6-trimethylphenyl)imidazol-2-ylidene

Base Information

Chemical Name:1-(1-(2,6-dimethylphenylimino)-2,2-dimethylpropyl)-3-(2,4,6-trimethylphenyl)imidazol-2-ylidene
CAS No.:1351994-92-7
Molecular Formula:C₂₅H₃₁N₃
Molecular Weight:373.541
Hs Code.:

Synonyms:1-(1-(2,6-dimethylphenylimino)-2,2-dimethylpropyl)-3-(2,4,6-trimethylphenyl)imidazol-2-ylidene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-(1-(2,6-dimethylphenylimino)-2,2-dimethylpropyl)-3-(2,4,6-trimethylphenyl)imidazol-2-ylidene

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Technology Process of 1-(1-(2,6-dimethylphenylimino)-2,2-dimethylpropyl)-3-(2,4,6-trimethylphenyl)imidazol-2-ylidene

There total 2 articles about 1-(1-(2,6-dimethylphenylimino)-2,2-dimethylpropyl)-3-(2,4,6-trimethylphenyl)imidazol-2-ylidene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 1-(1-(2,6-dimethylphenylimino)-2,2-dimethylpropyl)-3-(2,4,6-trimethylphenyl)imidazolium tetrafluoroborate

: 1351994-92-7
1-(1-(2,6-dimethylphenylimino)-2,2-dimethylpropyl)-3-(2,4,6-trimethylphenyl)imidazol-2-ylidene

Guidance literature:: With sodium hexamethyldisilazane; In tetrahydrofuran; at -78 - 20 ℃; for 2h;
DOI:10.1039/c1dt11565k

Reference yield:

: 57182-15-7
1-chloro-2,2-dimethyl-1-(2,6-dimethylphenylimino)propane

: 1351994-92-7
1-(1-(2,6-dimethylphenylimino)-2,2-dimethylpropyl)-3-(2,4,6-trimethylphenyl)imidazol-2-ylidene

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium tetrafluoroborate / acetonitrile / 48 h / 20 °C

1.2: 24 h

2.1: sodium hexamethyldisilazane / tetrahydrofuran / 2 h / -78 - 20 °C

With sodium tetrafluoroborate; sodium hexamethyldisilazane; In tetrahydrofuran; acetonitrile;
DOI:10.1039/c1dt11565k