8-(naphthalen-1-yl)e10,10-dioctyl-2,3-diphenyl-10Hindeno[1,2-g]quinoxaline

Base Information

Chemical Name:8-(naphthalen-1-yl)e10,10-dioctyl-2,3-diphenyl-10Hindeno[1,2-g]quinoxaline
CAS No.:1616933-80-2
Molecular Formula:C₅₃H₅₆N₂
Molecular Weight:721.041
Hs Code.:

Synonyms:8-(naphthalen-1-yl)e10,10-dioctyl-2,3-diphenyl-10Hindeno[1,2-g]quinoxaline

Suppliers and Price of 8-(naphthalen-1-yl)e10,10-dioctyl-2,3-diphenyl-10Hindeno[1,2-g]quinoxaline

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 8-(naphthalen-1-yl)e10,10-dioctyl-2,3-diphenyl-10Hindeno[1,2-g]quinoxaline

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 8-(naphthalen-1-yl)e10,10-dioctyl-2,3-diphenyl-10Hindeno[1,2-g]quinoxaline

There total 9 articles about 8-(naphthalen-1-yl)e10,10-dioctyl-2,3-diphenyl-10Hindeno[1,2-g]quinoxaline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 1612186-47-6
8-bromo-10,10-dioctyl-2,3-diphenyl-10H-indeno[1,2-g]quinoxaline

: 159087-45-3
4,4,5,5-tetramethyl-2-phenylethynyl-[1,3,2]dioxaborolane

: 1616933-80-2
8-(naphthalen-1-yl)e10,10-dioctyl-2,3-diphenyl-10Hindeno[1,2-g]quinoxaline

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; potassium carbonate; In water; toluene; at 90 ℃; for 24h; Inert atmosphere;
DOI:10.1016/j.dyepig.2014.04.042

Reference yield:

: 607-57-8
2-nitro-9H-fluorene

: 1616933-80-2
8-(naphthalen-1-yl)e10,10-dioctyl-2,3-diphenyl-10Hindeno[1,2-g]quinoxaline

Guidance literature:: Multi-step reaction with 9 steps

1.1: bromine / dichloromethane / 20 °C

2.1: potassium hydroxide / dimethyl sulfoxide / 0.5 h / 20 °C

2.2: 5 h / 20 °C

3.1: iron(III) chloride hexahydrate; pyrographite / methanol / 0.17 h / Inert atmosphere; Reflux

3.2: 2 h / Inert atmosphere; Reflux

4.1: acetic acid / 4 h / 20 °C

5.1: acetic acid; nitric acid / 0.5 h / 0 °C

6.1: sulfuric acid / ethanol / 2 h / 80 °C

7.1: iron(III) chloride hexahydrate; pyrographite / methanol / 0.17 h / Reflux; Inert atmosphere

7.2: 2 h / Reflux; Inert atmosphere

8.1: acetic acid; potassium carbonate / Reflux; Inert atmosphere

9.1: potassium carbonate; bis-triphenylphosphine-palladium(II) chloride / toluene; water / 24 h / 90 °C / Inert atmosphere

With bis-triphenylphosphine-palladium(II) chloride; iron(III) chloride hexahydrate; sulfuric acid; bromine; nitric acid; potassium carbonate; pyrographite; acetic acid; potassium hydroxide; In methanol; ethanol; dichloromethane; water; dimethyl sulfoxide; toluene; 9.1: |Suzuki Coupling;
DOI:10.1016/j.dyepig.2014.04.042

Reference yield:

: 1234321-63-1
2-bromo-7-nitro-9,9-dioctyl-9H-fluorene

: 1616933-80-2
8-(naphthalen-1-yl)e10,10-dioctyl-2,3-diphenyl-10Hindeno[1,2-g]quinoxaline

Guidance literature:: Multi-step reaction with 7 steps

1.1: iron(III) chloride hexahydrate; pyrographite / methanol / 0.17 h / Inert atmosphere; Reflux

1.2: 2 h / Inert atmosphere; Reflux

2.1: acetic acid / 4 h / 20 °C

3.1: acetic acid; nitric acid / 0.5 h / 0 °C

4.1: sulfuric acid / ethanol / 2 h / 80 °C

5.1: iron(III) chloride hexahydrate; pyrographite / methanol / 0.17 h / Reflux; Inert atmosphere

5.2: 2 h / Reflux; Inert atmosphere

6.1: acetic acid; potassium carbonate / Reflux; Inert atmosphere

7.1: potassium carbonate; bis-triphenylphosphine-palladium(II) chloride / toluene; water / 24 h / 90 °C / Inert atmosphere

With bis-triphenylphosphine-palladium(II) chloride; iron(III) chloride hexahydrate; sulfuric acid; nitric acid; potassium carbonate; pyrographite; acetic acid; In methanol; ethanol; water; toluene; 7.1: |Suzuki Coupling;
DOI:10.1016/j.dyepig.2014.04.042