7-bromo-9,9-dioctyl-9H-fluoren-2-amine

Base Information

Chemical Name:7-bromo-9,9-dioctyl-9H-fluoren-2-amine
CAS No.:1190425-63-8
Molecular Formula:C₂₉H₄₂BrN
Molecular Weight:484.563
Hs Code.:

Synonyms:7-bromo-9,9-dioctyl-9H-fluoren-2-amine

Suppliers and Price of 7-bromo-9,9-dioctyl-9H-fluoren-2-amine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 7-bromo-9,9-dioctyl-9H-fluoren-2-amine

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Technology Process of 7-bromo-9,9-dioctyl-9H-fluoren-2-amine

There total 1 articles about 7-bromo-9,9-dioctyl-9H-fluoren-2-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 302554-80-9
2-bromo-9,9-dioctyl-9H-fluorene

: 1190425-63-8
7-bromo-9,9-dioctyl-9H-fluoren-2-amine

Guidance literature:: Multi-step reaction with 2 steps

1: acetic acid; nitric acid / 4 h / 20 °C

2: iron; ammonium chloride / ethanol; water / 5 h / 85 °C / Inert atmosphere

With nitric acid; iron; ammonium chloride; acetic acid; In ethanol; water;
DOI:10.1039/c8ra05232h

Reference yield:

: 1190425-63-8
7-bromo-9,9-dioctyl-9H-fluoren-2-amine

: 1612186-57-8
4-(15,15-dioctyl-15H-dibenzo[a,c]indeno[1,2-i]phenazin-13-yl)-N,N-diphenylaniline

Guidance literature:: Multi-step reaction with 6 steps

1.1: acetic acid / 4 h / 20 °C

2.1: acetic acid; nitric acid / 0.5 h / 0 °C

3.1: sulfuric acid / ethanol / 2 h / 80 °C

4.1: iron(III) chloride hexahydrate; pyrographite / methanol / 0.17 h / Reflux; Inert atmosphere

4.2: 2 h / Reflux; Inert atmosphere

5.1: acetic acid; potassium carbonate / Reflux; Inert atmosphere

6.1: potassium carbonate; bis-triphenylphosphine-palladium(II) chloride / toluene; water / 24 h / 90 °C / Inert atmosphere

With bis-triphenylphosphine-palladium(II) chloride; iron(III) chloride hexahydrate; sulfuric acid; nitric acid; potassium carbonate; pyrographite; acetic acid; In methanol; ethanol; water; toluene; 6.1: |Suzuki Coupling;
DOI:10.1016/j.dyepig.2014.04.042

Reference yield:

: 1190425-63-8
7-bromo-9,9-dioctyl-9H-fluoren-2-amine

: 1612186-50-1
10,10-dioctyl-2,3,8-triphenyl-10H-indeno[1,2-g]quinoxaline

Guidance literature:: Multi-step reaction with 6 steps

1.1: acetic acid / 4 h / 20 °C

2.1: acetic acid; nitric acid / 0.5 h / 0 °C

3.1: sulfuric acid / ethanol / 2 h / 80 °C

4.1: iron(III) chloride hexahydrate; pyrographite / methanol / 0.17 h / Reflux; Inert atmosphere

4.2: 2 h / Reflux; Inert atmosphere

5.1: acetic acid; potassium carbonate / Reflux; Inert atmosphere

6.1: potassium carbonate; bis-triphenylphosphine-palladium(II) chloride / toluene; water / 24 h / 90 °C / Inert atmosphere

With bis-triphenylphosphine-palladium(II) chloride; iron(III) chloride hexahydrate; sulfuric acid; nitric acid; potassium carbonate; pyrographite; acetic acid; In methanol; ethanol; water; toluene; 6.1: |Suzuki Coupling;
DOI:10.1016/j.dyepig.2014.04.042