1,2-Ethanediamine,1,2-diphenyl-N1,N2-bis(phenylmethyl)-

Base Information

• Chemical Name: 1,2-Ethanediamine,1,2-diphenyl-N1,N2-bis(phenylmethyl)-
• CAS No.: 24431-19-4
• Molecular Formula: C₂₈H₂₈N₂
• Molecular Weight: 392.544
• Mol file: 24431-19-4.mol

Synonyms:1,2-Ethanediamine,1,2-diphenyl-N,N'-bis(phenylmethyl)- (9CI); Ethylenediamine,N,N'-dibenzyl-1,2-diphenyl- (6CI,8CI); NSC 167266

Chemical Property of 1,2-Ethanediamine,1,2-diphenyl-N1,N2-bis(phenylmethyl)-

Chemical Property:

Purity/Quality:

85.0-99.8% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1,2-Ethanediamine,1,2-diphenyl-N1,N2-bis(phenylmethyl)-

There total 39 articles about 1,2-Ethanediamine,1,2-diphenyl-N1,N2-bis(phenylmethyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

N-benzylidene benzylamine (780-25-6) → N,N'-dibenzyl-1,2-diphenyl-1,4-ethanediamine (24431-19-4,27549-71-9,27549-76-4)

Guidance literature:

With samarium diiodide; In tetrahydrofuran; Heating;

Reference yield: 82.0%

benzaldehyde (100-52-7) + benzylamine (100-46-9) → N,N'-dibenzyl-1,2-diphenyl-1,4-ethanediamine (24431-19-4,27549-71-9,27549-76-4) + dibenzylamine (103-49-1)

Guidance literature:

With water; potassium hydroxide; zinc; at 20 ℃; for 24h;

DOI:10.3762/bjoc.7.125

Reference yield: 66.0%

dibenzylamine (103-49-1) → N,N'-dibenzyl-1,2-diphenyl-1,4-ethanediamine (24431-19-4,27549-71-9,27549-76-4)

Guidance literature:

With cadmium(II) sulphide; In acetonitrile; at 20 ℃; for 24h; under 37.5038 Torr; Inert atmosphere; Irradiation;

DOI:10.1039/c2ob07053g

upstream raw materials:

N-Benzylidenebenzylamine N-oxide

N-benzylidene benzylamine

(E)-N-benzylidenebenzylamine

bromoacetic acid tert-butyl ester