4-(10-amino-3,4-dihydro-4,9,11,11a-tetraazadibenzo[cd,f]azulen-3-yl)-2-chlorophenol

Base Information

Chemical Name:4-(10-amino-3,4-dihydro-4,9,11,11a-tetraazadibenzo[cd,f]azulen-3-yl)-2-chlorophenol
CAS No.:1426667-52-8
Molecular Formula:C₁₉H₁₄ClN₅O
Molecular Weight:363.806
Hs Code.:

Synonyms:4-(10-amino-3,4-dihydro-4,9,11,11a-tetraazadibenzo[cd,f]azulen-3-yl)-2-chlorophenol

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Chemical Property of 4-(10-amino-3,4-dihydro-4,9,11,11a-tetraazadibenzo[cd,f]azulen-3-yl)-2-chlorophenol

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Technology Process of 4-(10-amino-3,4-dihydro-4,9,11,11a-tetraazadibenzo[cd,f]azulen-3-yl)-2-chlorophenol

There total 7 articles about 4-(10-amino-3,4-dihydro-4,9,11,11a-tetraazadibenzo[cd,f]azulen-3-yl)-2-chlorophenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.6%

: 1426666-85-4
methyl (3-(3-chloro-4-hydroxyphenyl)-3,4-dihydro-4,9,11,11a-tetraazadibenzo[cd,f]azulen-10-yl)carbamate

: 1426667-52-8
4-(10-amino-3,4-dihydro-4,9,11,11a-tetraazadibenzo[cd,f]azulen-3-yl)-2-chlorophenol

Guidance literature:: With water; sodium hydroxide; In methanol; for 5h; Reflux;

Reference yield:

: 1426663-88-8
methyl (4-(2-aminophenyl)pyrrolo[2,1-f][1,2,4]triazin-2-yl)carbamate

: 1426667-52-8
4-(10-amino-3,4-dihydro-4,9,11,11a-tetraazadibenzo[cd,f]azulen-3-yl)-2-chlorophenol

Guidance literature:: Multi-step reaction with 2 steps

1: acetic acid / 4 h / Reflux

2: water; sodium hydroxide / methanol / 5 h / Reflux

With water; acetic acid; sodium hydroxide; In methanol;

Reference yield:

: 628733-99-3
ethyl 1-amino-1H-pyrrole-2-carboxylate

: 1426667-52-8
4-(10-amino-3,4-dihydro-4,9,11,11a-tetraazadibenzo[cd,f]azulen-3-yl)-2-chlorophenol

Guidance literature:: Multi-step reaction with 6 steps

1: acetic acid / methanol / 16 h / 20 °C

2: sodium methylate / methanol / 16 h / 20 °C

3: N-benzyl-N,N,N-triethylammonium chloride; N,N-diethylaniline; trichlorophosphate / acetonitrile / 15 h / 80 °C

4: bis-triphenylphosphine-palladium(II) chloride; sodium carbonate / water; N,N-dimethyl-formamide / 2 h / 80 °C / Inert atmosphere

5: acetic acid / 4 h / Reflux

6: water; sodium hydroxide / methanol / 5 h / Reflux

With bis-triphenylphosphine-palladium(II) chloride; N-benzyl-N,N,N-triethylammonium chloride; water; sodium methylate; sodium carbonate; acetic acid; N,N-diethylaniline; sodium hydroxide; trichlorophosphate; In methanol; water; N,N-dimethyl-formamide; acetonitrile;