2-10-formylpteroyl)amino>dodecanedioic acid dimethyl ester

Base Information

Chemical Name:2-10-formylpteroyl)amino>dodecanedioic acid dimethyl ester
CAS No.:113976-37-7
Molecular Formula:C₂₉H₃₈N₈O₆
Molecular Weight:594.671
Hs Code.:

2-<N-(4-amino-4-deoxy-N<sup>10</sup>-formylpteroyl)amino>dodecanedioic acid dimethyl ester

Synonyms:2-10-formylpteroyl)amino>dodecanedioic acid dimethyl ester

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Chemical Property of 2-10-formylpteroyl)amino>dodecanedioic acid dimethyl ester

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Technology Process of 2-10-formylpteroyl)amino>dodecanedioic acid dimethyl ester

There total 5 articles about 2-10-formylpteroyl)amino>dodecanedioic acid dimethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

: 95485-01-1
p-nitrophenyl 4-amino-4-deoxy-N¹⁰-formylpteroate

: 5686-30-6
2-Amino-dodecanedioic acid dimethyl ester; hydrochloride

: 113976-37-7
2-10-formylpteroyl)amino>dodecanedioic acid dimethyl ester

Guidance literature:: With triethylamine; In various solvent(s); at 55 ℃; for 114h;
DOI:10.1021/jm00402a014

Reference yield:

: 3903-40-0
12-methoxy-12-oxododecanoic acid

: 113976-37-7
2-10-formylpteroyl)amino>dodecanedioic acid dimethyl ester

Guidance literature:: Multi-step reaction with 6 steps

1: SOCl₂ / dimethylformamide / 3 h / Heating

2: Br₂, I₂ / SOCl₂; dimethylformamide / 4 h / Irradiation

3: 3.5 h / Ambient temperature

4: NaN₃ / ethanol / 15 h / Heating

5: H₂, aq. HCl / Pd-C / ethanol / 17 h

6: 46 percent / Et₃N / various solvent(s) / 114 h / 55 °C

With hydrogenchloride; thionyl chloride; sodium azide; hydrogen; bromine; iodine; triethylamine; palladium on activated charcoal; In thionyl chloride; ethanol; N,N-dimethyl-formamide;
DOI:10.1021/jm00402a014

Reference yield:

: 113976-41-3
α-Brom-dodecandisaeure-dimethylester

: 113976-37-7
2-10-formylpteroyl)amino>dodecanedioic acid dimethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: NaN₃ / ethanol / 15 h / Heating

2: H₂, aq. HCl / Pd-C / ethanol / 17 h

3: 46 percent / Et₃N / various solvent(s) / 114 h / 55 °C

With hydrogenchloride; sodium azide; hydrogen; triethylamine; palladium on activated charcoal; In ethanol;
DOI:10.1021/jm00402a014