(2,6-dimethyl-4-triisopropylsilanyloxyphenyl)-(4-methoxymethoxyphenyl)methanol

Base Information

Chemical Name:(2,6-dimethyl-4-triisopropylsilanyloxyphenyl)-(4-methoxymethoxyphenyl)methanol
CAS No.:852949-17-8
Molecular Formula:C₂₆H₄₀O₄Si
Molecular Weight:444.687
Hs Code.:

Synonyms:(2,6-dimethyl-4-triisopropylsilanyloxyphenyl)-(4-methoxymethoxyphenyl)methanol

Suppliers and Price of (2,6-dimethyl-4-triisopropylsilanyloxyphenyl)-(4-methoxymethoxyphenyl)methanol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of (2,6-dimethyl-4-triisopropylsilanyloxyphenyl)-(4-methoxymethoxyphenyl)methanol

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

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Technology Process of (2,6-dimethyl-4-triisopropylsilanyloxyphenyl)-(4-methoxymethoxyphenyl)methanol

There total 1 articles about (2,6-dimethyl-4-triisopropylsilanyloxyphenyl)-(4-methoxymethoxyphenyl)methanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6515-21-5
4-methoxymethoxy-benzaldehyde

: 328236-43-7
(4-bromo-3,5-dimethylphenoxy)triisopropylsilane

: 852949-17-8
(2,6-dimethyl-4-triisopropylsilanyloxyphenyl)-(4-methoxymethoxyphenyl)methanol

Guidance literature:: (4-bromo-3,5-dimethylphenoxy)triisopropylsilane; With n-butyllithium; In tetrahydrofuran; at -78 ℃; for 1h;

4-methoxymethoxy-benzaldehyde; In tetrahydrofuran; at -78 - 20 ℃; for 1h;

Reference yield: 41.5%

: 852949-17-8
(2,6-dimethyl-4-triisopropylsilanyloxyphenyl)-(4-methoxymethoxyphenyl)methanol

: 852949-18-9
4-(2,6-dimethyl-4-triisopropylsilanyloxybenzyl)-methoxymethoxybenzene

Guidance literature:: With hydrogen; palladium on activated charcoal; In acetic acid; ethyl acetate; at 20 ℃; for 5h; under 760.051 Torr;

Reference yield:

: 852949-17-8
(2,6-dimethyl-4-triisopropylsilanyloxyphenyl)-(4-methoxymethoxyphenyl)methanol

: 852949-20-3
5-(4-hydroxy-2,6-dimethylbenzyl)-2-methoxymethoxybenzaldehyde

Guidance literature:: Multi-step reaction with 3 steps

1.1: hydrogen / palladium on activated charcoal / acetic acid; ethyl acetate / 5 h / 20 °C / 760.05 Torr

2.1: n-butyllithium; N,N,N,N,-tetramethylethylenediamine / tetrahydrofuran; diethyl ether / 1 h / -20 - 0 °C

2.2: 2 h / 0 °C

3.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 0 - 20 °C

With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; tetrabutyl ammonium fluoride; hydrogen; palladium on activated charcoal; In tetrahydrofuran; diethyl ether; acetic acid; ethyl acetate;