p-nitrophenyl N^α-(9-fluorenylmethyloxycarbonyl)-N^ε-(benzyloxycarbonyl)-L-lysinate

Base Information

• Chemical Name: p-nitrophenyl N^α-(9-fluorenylmethyloxycarbonyl)-N^ε-(benzyloxycarbonyl)-L-lysinate
• CAS No.: 122903-72-4
• Molecular Formula: C₃₅H₃₃N₃O₈
• Molecular Weight: 623.662

Synonyms:p-nitrophenyl N^α-(9-fluorenylmethyloxycarbonyl)-N^ε-(benzyloxycarbonyl)-L-lysinate

Chemical Property of p-nitrophenyl N^α-(9-fluorenylmethyloxycarbonyl)-N^ε-(benzyloxycarbonyl)-L-lysinate

Chemical Property:

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Technology Process of p-nitrophenyl N^α-(9-fluorenylmethyloxycarbonyl)-N^ε-(benzyloxycarbonyl)-L-lysinate

There total 1 articles about p-nitrophenyl N^α-(9-fluorenylmethyloxycarbonyl)-N^ε-(benzyloxycarbonyl)-L-lysinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

Fmoc-Lys(Z)-OH (86060-82-4,110990-07-3) + 4-Nitrophenyl chloroformate (7693-46-1) → p-nitrophenyl Nα-(9-fluorenylmethyloxycarbonyl)-Nε-(benzyloxycarbonyl)-L-lysinate (122903-72-4)

Guidance literature:

With 0,2,4-dichlorophenyl-0-methylisopropylamidothiophosphate; Etifelmin; In dichloromethane; for 1.5h; Ambient temperature;

DOI:10.1021/jo00284a031

Reference yield: 87.0%

p-nitrophenyl Nα-(9-fluorenylmethyloxycarbonyl)-Nε-(benzyloxycarbonyl)-L-lysinate (122903-72-4) + Nα-ε-<<2-(trimethylsilyl)ethoxy>carbonyl>-L-lysyl>-Nε-<<2-(trimethylsilyl)ethoxy>carbonyl>-L-lysine (122903-63-3) → Nα-α-α-(9-fluorenylmethyloxycarbonyl)-Nε-(benzyloxycarbonyl)-L-lysyl>-Nε-<<2-(trimethylsilyl)ethoxy>carbonyl>-L-lysyl>-Nε-<<2-(trimethylsilyl)ethoxy>carbonyl>-L-lysine (122903-73-5)

Guidance literature:

With dmap; Etifelmin; In dichloromethane; for 72h;

DOI:10.1021/jo00284a031

Reference yield: 57.0%

p-nitrophenyl Nα-(9-fluorenylmethyloxycarbonyl)-Nε-(benzyloxycarbonyl)-L-lysinate (122903-72-4) + Nα-α-ε-<<2-(trimethylsilyl)ethoxy>carbonyl>-L-lysyl>-Nε-<<2-(trimethylsilyl)ethoxy>carbonyl>-L-lysyl>-Nε-<<2-(trimethylsilyl)ethoxy>carbonyl>-L-lysine (122903-64-4) → Nα-α-α-α-(9-fluorenylmethyloxycarbonyl)-Nε-(benzyloxycarbonyl)-L-lysyl>-Nε-<<2-(trimethylsilyl)ethoxy>carbonyl>-L-lysyl>-Nε-<<2-(trimethylsilyl)ethoxy>carbonyl>-L-lysyl>-Nε-<<2-(trimethylsilyl)ethoxy>carbonyl>-L-lysine (122903-75-7)

Guidance literature:

With Etifelmin; In dichloromethane; for 60h;

DOI:10.1021/jo00284a031

upstream raw materials:

Fmoc-Lys(Z)-OH

4-Nitrophenyl chloroformate

Downstream raw materials:

N^α-α-α-α-(9-fluorenylmethyloxycarbonyl)-N^ε-(benzyloxycarbonyl)-L-lysyl>-N^ε-<<2-(trimethylsilyl)ethoxy>carbonyl>-L-lysyl>-N^ε-<<2-(trimethylsilyl)ethoxy>carbonyl>-L-lysyl>-N^ε-<<2-(trimethylsilyl)ethoxy>carbonyl>-L-lysine

N^α-α-α-(9-fluorenylmethyloxycarbonyl)-N^ε-(benzyloxycarbonyl)-L-lysyl>-N^ε-<<2-(trimethylsilyl)ethoxy>carbonyl>-L-lysyl>-N^ε-<<2-(trimethylsilyl)ethoxy>carbonyl>-L-lysine

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