2,3,5,6-tetra-O-benzoyl-D-galactofuranoside N-phenyltrifluoroacetimidate

Base Information

Chemical Name:2,3,5,6-tetra-O-benzoyl-D-galactofuranoside N-phenyltrifluoroacetimidate
CAS No.:1260145-53-6
Molecular Formula:C₄₂H₃₂F₃NO₁₀
Molecular Weight:767.712
Hs Code.:

Synonyms:2,3,5,6-tetra-O-benzoyl-D-galactofuranoside N-phenyltrifluoroacetimidate

Suppliers and Price of 2,3,5,6-tetra-O-benzoyl-D-galactofuranoside N-phenyltrifluoroacetimidate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2,3,5,6-tetra-O-benzoyl-D-galactofuranoside N-phenyltrifluoroacetimidate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2,3,5,6-tetra-O-benzoyl-D-galactofuranoside N-phenyltrifluoroacetimidate

There total 2 articles about 2,3,5,6-tetra-O-benzoyl-D-galactofuranoside N-phenyltrifluoroacetimidate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 61881-19-4
2,2,2-trifluoro-N-phenyl-acetimidoyl chloride

: 5531-48-6,5531-49-7,5531-50-0,5595-67-5,5636-01-1,108223-94-5
2,3,5,6-tetra-O-benzoyl-D-galactofuranose

: 1260145-53-6
2,3,5,6-tetra-O-benzoyl-D-galactofuranoside N-phenyltrifluoroacetimidate

Guidance literature:: With caesium carbonate; In dichloromethane; at 23 ℃; for 1h; Inert atmosphere;
DOI:10.1021/ja1087375

Reference yield:

: 1033560-31-4
4-methylphenyl 2,3,5,6-tetra-O-benzoyl-1-thio-β-D-galactofuranoside

: 1260145-53-6
2,3,5,6-tetra-O-benzoyl-D-galactofuranoside N-phenyltrifluoroacetimidate

Guidance literature:: Multi-step reaction with 2 steps

1: N-Bromosuccinimide; water / ethyl acetate / 12 h / 23 °C / Inert atmosphere

2: caesium carbonate / dichloromethane / 1 h / 23 °C / Inert atmosphere

With N-Bromosuccinimide; water; caesium carbonate; In dichloromethane; ethyl acetate;
DOI:10.1021/ja1087375

Reference yield: 90.0%

: 1260145-53-6
2,3,5,6-tetra-O-benzoyl-D-galactofuranoside N-phenyltrifluoroacetimidate

: 1260145-58-1
tert-butyldimethylsilyl 3-O-acetyl-2-azido-4-(benzyloxycarbonyl)amino-2,4,6-trideoxy-α-D-galactopyranosyl-(1->4)-2-azido-6-O-benzyl-2-deoxy-β-D-galactopyranoside

: 1260145-60-5
tert-butyldimethylsilyl 3-O-acetyl-2-azido-4-(benzyloxycarbonyl)amino-2,4,6-trideoxy-α-D-galactopyranosyl-(1->4)-[2,3,5,6-tetra-O-benzoyl-β-D-galactofuranosyl-(1->3)]-2-azido-6-O-benzyl-2-deoxy-β-D-galactopyranoside

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at -30 ℃; for 1h; Inert atmosphere;
DOI:10.1021/ja1087375