isopropyl 2-O-benzoyl-3-O-[2-azido-4,6-O-benzylidene-3-O-(2,3,5,6-tetra-O-benzoyl-β-D-galactofuranosyl)-2-deoxy-α-D-galactopyranosyl]-4,6-O-[1-(R)-(methoxycarbonyl)-ethylidene]-β-D-galactopyranoside

Base Information

Chemical Name:isopropyl 2-O-benzoyl-3-O-[2-azido-4,6-O-benzylidene-3-O-(2,3,5,6-tetra-O-benzoyl-β-D-galactofuranosyl)-2-deoxy-α-D-galactopyranosyl]-4,6-O-[1-(R)-(methoxycarbonyl)-ethylidene]-β-D-galactopyranoside
CAS No.:936324-90-2
Molecular Formula:C₆₇H₆₅N₃O₂₂
Molecular Weight:1264.26
Hs Code.:

isopropyl 2-O-benzoyl-3-O-[2-azido-4,6-O-benzylidene-3-O-(2,3,5,6-tetra-O-benzoyl-β-D-galactofuranosyl)-2-deoxy-α-D-galactopyranosyl]-4,6-O-[1-(R)-(methoxycarbonyl)-ethylidene]-β-D-galactopyranoside

Synonyms:isopropyl 2-O-benzoyl-3-O-[2-azido-4,6-O-benzylidene-3-O-(2,3,5,6-tetra-O-benzoyl-β-D-galactofuranosyl)-2-deoxy-α-D-galactopyranosyl]-4,6-O-[1-(R)-(methoxycarbonyl)-ethylidene]-β-D-galactopyranoside

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Chemical Property of isopropyl 2-O-benzoyl-3-O-[2-azido-4,6-O-benzylidene-3-O-(2,3,5,6-tetra-O-benzoyl-β-D-galactofuranosyl)-2-deoxy-α-D-galactopyranosyl]-4,6-O-[1-(R)-(methoxycarbonyl)-ethylidene]-β-D-galactopyranoside

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Technology Process of isopropyl 2-O-benzoyl-3-O-[2-azido-4,6-O-benzylidene-3-O-(2,3,5,6-tetra-O-benzoyl-β-D-galactofuranosyl)-2-deoxy-α-D-galactopyranosyl]-4,6-O-[1-(R)-(methoxycarbonyl)-ethylidene]-β-D-galactopyranoside

There total 11 articles about isopropyl 2-O-benzoyl-3-O-[2-azido-4,6-O-benzylidene-3-O-(2,3,5,6-tetra-O-benzoyl-β-D-galactofuranosyl)-2-deoxy-α-D-galactopyranosyl]-4,6-O-[1-(R)-(methoxycarbonyl)-ethylidene]-β-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 936324-85-5
isopropyl 2-O-benzoyl-4,6-O-[1-(R)-(methoxycarbonyl)-ethylidene]-β-D-galactopyranoside

: 548477-84-5
phenyl 3-O-(2,3,5,6-tetra-O-benzoyl-α-D-galactofuranosyl)-2-azido-4,6-O-benzylidene-2-deoxy-1-seleno-α-D-galactopyranoside

: 936324-90-2
isopropyl 2-O-benzoyl-3-O-[2-azido-4,6-O-benzylidene-3-O-(2,3,5,6-tetra-O-benzoyl-β-D-galactofuranosyl)-2-deoxy-α-D-galactopyranosyl]-4,6-O-[1-(R)-(methoxycarbonyl)-ethylidene]-β-D-galactopyranoside

Guidance literature:: With N-iodo-succinimide; trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at 0 - 20 ℃; for 1h;
DOI:10.1016/j.tetlet.2007.02.067

Reference yield: 62.0%

: C₁₃H₁₅N₃O₅

: 936324-85-5
isopropyl 2-O-benzoyl-4,6-O-[1-(R)-(methoxycarbonyl)-ethylidene]-β-D-galactopyranoside

: 5531-48-6,5531-49-7,5531-50-0,5595-67-5,5636-01-1,108223-94-5
2,3,5,6-tetra-O-benzoyl-D-galactofuranose

: 936324-90-2
isopropyl 2-O-benzoyl-3-O-[2-azido-4,6-O-benzylidene-3-O-(2,3,5,6-tetra-O-benzoyl-β-D-galactofuranosyl)-2-deoxy-α-D-galactopyranosyl]-4,6-O-[1-(R)-(methoxycarbonyl)-ethylidene]-β-D-galactopyranoside

Guidance literature:: C₁₃H₁₅N₃O₅; 2,3,5,6-tetra-O-benzoyl-D-galactofuranose; With trifluoromethylsulfonic anhydride; 1,1'-sulfinylbisbenzene; 2,4,5-tri-tert-butylpyrimidine; In 1,4-dioxane; dichloromethane; at -40 - 20 ℃; for 16h;

isopropyl 2-O-benzoyl-4,6-O-[1-(R)-(methoxycarbonyl)-ethylidene]-β-D-galactopyranoside; With trifluoromethylsulfonic anhydride; 2,4,5-tri-tert-butylpyrimidine; In 1,4-dioxane; dichloromethane; at -40 - 20 ℃; for 16h; Further stages.;
DOI:10.1016/j.tetlet.2007.02.067

Reference yield: 57.0%

: 1260145-54-7
isopropyl 2-azido-4,6-O-benzylidene-2-deoxy-α-D-galactopyranosyl-(1->3)-2-O-benzoyl-4,6-O-[1-(R)-(methoxycarbonyl)ethylidene]-β-D-galactopyranoside

: 1260145-53-6
2,3,5,6-tetra-O-benzoyl-D-galactofuranoside N-phenyltrifluoroacetimidate

: 936324-90-2
isopropyl 2-O-benzoyl-3-O-[2-azido-4,6-O-benzylidene-3-O-(2,3,5,6-tetra-O-benzoyl-β-D-galactofuranosyl)-2-deoxy-α-D-galactopyranosyl]-4,6-O-[1-(R)-(methoxycarbonyl)-ethylidene]-β-D-galactopyranoside

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at -60 ℃; for 1h; Inert atmosphere;
DOI:10.1021/ja1087375