N-(3-Bromo-propyl)-4-methyl-N-[3-methyl-4-(4-nitro-benzenesulfonyl)-phenyl]-benzenesulfonamide

Base Information

Chemical Name:N-(3-Bromo-propyl)-4-methyl-N-[3-methyl-4-(4-nitro-benzenesulfonyl)-phenyl]-benzenesulfonamide
CAS No.:176512-36-0
Molecular Formula:C₂₃H₂₃BrN₂O₆S₂
Molecular Weight:567.481
Hs Code.:

Synonyms:N-(3-Bromo-propyl)-4-methyl-N-[3-methyl-4-(4-nitro-benzenesulfonyl)-phenyl]-benzenesulfonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(3-Bromo-propyl)-4-methyl-N-[3-methyl-4-(4-nitro-benzenesulfonyl)-phenyl]-benzenesulfonamide

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Technology Process of N-(3-Bromo-propyl)-4-methyl-N-[3-methyl-4-(4-nitro-benzenesulfonyl)-phenyl]-benzenesulfonamide

There total 4 articles about N-(3-Bromo-propyl)-4-methyl-N-[3-methyl-4-(4-nitro-benzenesulfonyl)-phenyl]-benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 176512-31-5
4-amino-2-methyl-4'-nitrodiphenyl sulfide

: 176512-36-0
N-(3-Bromo-propyl)-4-methyl-N-[3-methyl-4-(4-nitro-benzenesulfonyl)-phenyl]-benzenesulfonamide

Guidance literature:: With dihydrogen peroxide; In acetic acid; at 65 ℃;
DOI:10.1002/ardp.19963290309

Reference yield:

: 176512-23-5
3-methyl-4-(4-nitrophenylthio)aniline

: 176512-36-0
N-(3-Bromo-propyl)-4-methyl-N-[3-methyl-4-(4-nitro-benzenesulfonyl)-phenyl]-benzenesulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / 3 h

2: 74 percent / NaI, CuI, aq. KOH / ethanol / Heating

3: 92 percent / 30percent H₂O₂ / acetic acid / 65 °C

With potassium hydroxide; copper(l) iodide; dihydrogen peroxide; sodium iodide; In pyridine; ethanol; acetic acid;
DOI:10.1002/ardp.19963290309

Reference yield:

: 98-59-9
p-toluenesulfonyl chloride

: 176512-36-0
N-(3-Bromo-propyl)-4-methyl-N-[3-methyl-4-(4-nitro-benzenesulfonyl)-phenyl]-benzenesulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / 3 h

2: 74 percent / NaI, CuI, aq. KOH / ethanol / Heating

3: 92 percent / 30percent H₂O₂ / acetic acid / 65 °C

With potassium hydroxide; copper(l) iodide; dihydrogen peroxide; sodium iodide; In pyridine; ethanol; acetic acid;
DOI:10.1002/ardp.19963290309