4-Methyl-N-[3-methyl-4-(4-nitro-phenylsulfanyl)-phenyl]-benzenesulfonamide

Base Information

• Chemical Name: 4-Methyl-N-[3-methyl-4-(4-nitro-phenylsulfanyl)-phenyl]-benzenesulfonamide
• CAS No.: 176512-26-8
• Molecular Formula: C₂₀H₁₈N₂O₄S₂
• Molecular Weight: 414.506
• Mol file: 176512-26-8.mol

Synonyms:4-Methyl-N-[3-methyl-4-(4-nitro-phenylsulfanyl)-phenyl]-benzenesulfonamide

Chemical Property of 4-Methyl-N-[3-methyl-4-(4-nitro-phenylsulfanyl)-phenyl]-benzenesulfonamide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of 4-Methyl-N-[3-methyl-4-(4-nitro-phenylsulfanyl)-phenyl]-benzenesulfonamide

There total 1 articles about 4-Methyl-N-[3-methyl-4-(4-nitro-phenylsulfanyl)-phenyl]-benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-methyl-4-(4-nitrophenylthio)aniline (176512-23-5) + p-toluenesulfonyl chloride (98-59-9) → 4-Methyl-N-[3-methyl-4-(4-nitro-phenylsulfanyl)-phenyl]-benzenesulfonamide (176512-26-8)

Guidance literature:

In pyridine; for 3h; Yield given;

DOI:10.1002/ardp.19963290309

Reference yield: 74.0%

1,3-dibromo-propane (109-64-8) + 4-Methyl-N-[3-methyl-4-(4-nitro-phenylsulfanyl)-phenyl]-benzenesulfonamide (176512-26-8) → 4-amino-2-methyl-4'-nitrodiphenyl sulfide (176512-31-5)

Guidance literature:

With potassium hydroxide; copper(l) iodide; sodium iodide; In ethanol; Heating;

DOI:10.1002/ardp.19963290309

Reference yield: 73.0%

propyl bromide (106-94-5) + 4-Methyl-N-[3-methyl-4-(4-nitro-phenylsulfanyl)-phenyl]-benzenesulfonamide (176512-26-8) → 2-methyl-4-(N-propyl-N-tosyl)-amino-4'-nitrodiphenyl sulfide (176512-28-0)

Guidance literature:

With sodium hydroxide; copper(l) iodide; sodium iodide; In ethanol; for 17h; Heating;

DOI:10.1002/ardp.19963290309

upstream raw materials:

3-methyl-4-(4-nitrophenylthio)aniline

p-toluenesulfonyl chloride

Downstream raw materials:

2-methyl-4-(N-propyl-N-tosyl)-amino-4'-nitrodiphenyl sulfide

4-amino-2-methyl-4'-nitrodiphenyl sulfide

4'-amino-2-methyl-4-n-propylamino-diphenylsulfone

2-methyl-4'-nitro-4-n-propylamino-diphenylsulfone